Technology Process of N-(6-Phenylsulfinyl-5-indanyl)-methansulfonamid
There total 9 articles about N-(6-Phenylsulfinyl-5-indanyl)-methansulfonamid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
In
acetone;
for 30h;
Heating;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 50 percent / cc H2SO4, HNO3 / 1./ 0.5 h. 2./ 1 h. room temp.
2: 1./ cc H2SO4, NaNO2, acetic acid, 2./ CuBr, NaBr, 16percent HBr / 1./ water, 1 h. 3-5 deg C.
3: 50 percent / CuCl, K2CO3 / pyridine / 3 h / Heating
4: 83 percent / hydrazine hydrate / Raney-nickel / ethanol / 1 h / Heating
5: 81 percent / pyridine / 1./ 3 h. 0 deg C. 2./ room temp.
6: 63 percent / 30percent H2O2 / acetone / 30 h / Heating
With
pyridine; sulfuric acid; hydrogen bromide; dihydrogen peroxide; nitric acid; potassium carbonate; hydrazine hydrate; acetic acid; sodium bromide; copper(l) chloride; copper(I) bromide; sodium nitrite;
nickel;
In
pyridine; ethanol; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 37 percent / HNO3 / 0.25 h / 0 - 5 °C
2: 50 percent / CuCl, K2CO3 / pyridine / 3 h / Heating
3: 83 percent / hydrazine hydrate / Raney-nickel / ethanol / 1 h / Heating
4: 81 percent / pyridine / 1./ 3 h. 0 deg C. 2./ room temp.
5: 63 percent / 30percent H2O2 / acetone / 30 h / Heating
With
pyridine; dihydrogen peroxide; nitric acid; potassium carbonate; hydrazine hydrate; copper(l) chloride;
nickel;
In
pyridine; ethanol; acetone;
