ethyl methylphosphinate

Base Information

Chemical Name:ethyl methylphosphinate
CAS No.:80953-52-2
Molecular Formula:C₁₂H₁₇O₄P
Molecular Weight:256.238
Hs Code.:

ethyl methyl<o-(acetoxymethyl)phenyl>phosphinate

Synonyms:ethyl methylphosphinate

Suppliers and Price of ethyl methylphosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl methylphosphinate

Chemical Property:

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Technology Process of ethyl methylphosphinate

There total 2 articles about ethyl methylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 15715-41-0
methyldiethoxyphosphine

: 80953-51-1
(2-iodophenyl)methyl acetate

: 80953-52-2
ethyl methylphosphinate

Guidance literature:: With nickel dichloride; at 165 - 175 ℃; for 0.5h;
DOI:10.1021/jo00348a013

Reference yield:

: 5159-41-1
2-iodobenzyl alcohol

: 80953-52-2
ethyl methylphosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 2 h / Heating

2: 81 percent / NiCl₂ / 0.5 h / 165 - 175 °C

With nickel dichloride;
DOI:10.1021/jo00348a013

Reference yield:

: 80953-52-2
ethyl methylphosphinate

: 80953-53-3
methylphosphinic acid sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 10percent HClO₄ / H₂O / 0.5 h / Heating

2: 93 percent / NaHCO₃ / H₂O / 2 h / Heating

With perchloric acid; sodium hydrogencarbonate; In water;
DOI:10.1021/jo00348a013