(R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate

Base Information

Chemical Name:(R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate
CAS No.:1040272-09-0
Molecular Formula:C₂₄H₂₆O₅
Molecular Weight:394.467
Hs Code.:

Synonyms:(R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate

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Chemical Property of (R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate

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Technology Process of (R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate

There total 2 articles about (R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1040272-07-8
C₂₆H₂₄O₈

: 26902-24-9
3-(benzyloxy)-3-methyl-1-butene

: 1040272-09-0
(R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; at 23 ℃; Inert atmosphere;
DOI:10.1002/chem.200701998

Reference yield: 61.0%

: 1040272-04-5
(R)-benzyl 2-allyl-4-oxooxetane-2-carboxylate

: 26902-24-9
3-(benzyloxy)-3-methyl-1-butene

: 1040272-09-0
(R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate

: 1040272-07-8
C₂₆H₂₄O₈

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 23 ℃; for 49h; Inert atmosphere;
DOI:10.1002/chem.200701998

Reference yield: 85.0%

: 1040272-09-0
(R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate

: 1040272-12-5
(R,E)-2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylic acid

Guidance literature:: (R,E)-benzyl 2-(4-(benzyloxy)-4-methylpent-2-enyl)-4-oxooxetane-2-carboxylate; With triethylsilane; triethylamine; palladium diacetate; In dichloromethane; at 23 ℃; for 1h; Inert atmosphere;

With water; ammonium chloride; In dichloromethane;