(1,8-diamino-3,6,10,13,16,19-hexaazabicyclo[6.6.6]eicosane)chromium(III) chloride monohydrate

Base Information

Chemical Name:(1,8-diamino-3,6,10,13,16,19-hexaazabicyclo[6.6.6]eicosane)chromium(III) chloride monohydrate
CAS No.:99583-52-5
Molecular Formula:C₁₄H₃₄CrN₈*3Cl*H₂O
Molecular Weight:490.848
Hs Code.:

Synonyms:(1,8-diamino-3,6,10,13,16,19-hexaazabicyclo[6.6.6]eicosane)chromium(III) chloride monohydrate

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Chemical Property of (1,8-diamino-3,6,10,13,16,19-hexaazabicyclo[6.6.6]eicosane)chromium(III) chloride monohydrate

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Technology Process of (1,8-diamino-3,6,10,13,16,19-hexaazabicyclo[6.6.6]eicosane)chromium(III) chloride monohydrate

There total 1 articles about (1,8-diamino-3,6,10,13,16,19-hexaazabicyclo[6.6.6]eicosane)chromium(III) chloride monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10025-73-7,16284-59-6
chromium(III) chloride

: 91002-72-1
diamsar

: 99583-52-5
(1,8-diamino-3,6,10,13,16,19-hexaazabicyclo[6.6.6]eicosane)chromium(III) chloride monohydrate

Guidance literature:: With Zn; H₂O; In dimethyl sulfoxide; Warming of DMSO soln. of org. ligand in a steam bath, then addn. of Zn powder and anhyd. CrCl3, and gentle warming (5 min). Addn. of resulting green-yellow soln. to large volume of H2O.; Filtn., sorbing of filtrate on column, washing (H2O, HCl), elution (HCl). Collecting of major yellow band, evapn. to dryness, redissolving of yellow solid in H2O, chromy. Evapn. of solvent, crystn. (aq. propan-2-ol), addn. of LiOH, elem. anal.;