6-(perfluorophenyl)-2,3-dihydrobenzo[b][1,4]dioxin

Base Information

• Chemical Name: 6-(perfluorophenyl)-2,3-dihydrobenzo[b][1,4]dioxin
• CAS No.: 1206164-16-0
• Molecular Formula: C₁₄H₇F₅O₂
• Molecular Weight: 302.2
• Mol file: 1206164-16-0.mol

Synonyms:6-(perfluorophenyl)-2,3-dihydrobenzo[b][1,4]dioxin

Chemical Property of 6-(perfluorophenyl)-2,3-dihydrobenzo[b][1,4]dioxin

Chemical Property:

Purity/Quality:

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Technology Process of 6-(perfluorophenyl)-2,3-dihydrobenzo[b][1,4]dioxin

There total 1 articles about 6-(perfluorophenyl)-2,3-dihydrobenzo[b][1,4]dioxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

6-iodo-1,4-benzodioxane (57744-67-9) + potassium 2,3,4,5,6-pentafluorobenzoate (58521-27-0) → 6-(perfluorophenyl)-2,3-dihydrobenzo[b][1,4]dioxin (1206164-16-0)

Guidance literature:

With copper(l) iodide; In diethylene glycol dimethyl ether; at 130 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.200904916

upstream raw materials:

6-iodo-1,4-benzodioxane

potassium 2,3,4,5,6-pentafluorobenzoate

Refernces