S-3-((2-(benzyloxycarbonylamino)-2-methylpropyl)(methyl)amino)-3-oxopropyl ethanethioate

Base Information

Chemical Name:S-3-((2-(benzyloxycarbonylamino)-2-methylpropyl)(methyl)amino)-3-oxopropyl ethanethioate
CAS No.:1037832-88-4
Molecular Formula:C₁₈H₂₆N₂O₄S
Molecular Weight:366.481
Hs Code.:

Synonyms:S-3-((2-(benzyloxycarbonylamino)-2-methylpropyl)(methyl)amino)-3-oxopropyl ethanethioate

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Chemical Property of S-3-((2-(benzyloxycarbonylamino)-2-methylpropyl)(methyl)amino)-3-oxopropyl ethanethioate

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Technology Process of S-3-((2-(benzyloxycarbonylamino)-2-methylpropyl)(methyl)amino)-3-oxopropyl ethanethioate

There total 4 articles about S-3-((2-(benzyloxycarbonylamino)-2-methylpropyl)(methyl)amino)-3-oxopropyl ethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 41345-70-4
3-acetylsulfanyl-propionic acid

: 1037832-87-3
benzyl-2-methyl-1-(methylamino)propan-2-ylcarbamate

: 1037832-88-4
S-3-((2-(benzyloxycarbonylamino)-2-methylpropyl)(methyl)amino)-3-oxopropyl ethanethioate

Guidance literature:: 3-acetylsulfanyl-propionic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 0.333333h;

benzyl-2-methyl-1-(methylamino)propan-2-ylcarbamate; In tetrahydrofuran; for 2h; Heating / reflux;

Reference yield:

: 1037832-90-8
C₁₃H₁₈N₂O₃

: 1037832-88-4
S-3-((2-(benzyloxycarbonylamino)-2-methylpropyl)(methyl)amino)-3-oxopropyl ethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 °C

1.2: 1 h

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 0.33 h / 20 °C

2.2: 2 h / Heating / reflux

With dimethylsulfide borane complex; 1,1'-carbonyldiimidazole; In tetrahydrofuran;

Reference yield:

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 1037832-88-4
S-3-((2-(benzyloxycarbonylamino)-2-methylpropyl)(methyl)amino)-3-oxopropyl ethanethioate

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol / -78 °C

1.2: 0 °C

2.1: hydrogenchloride / water / 2 h / 20 °C

3.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h

4.1: dimethylsulfide borane complex / tetrahydrofuran / 0 °C

4.2: 1 h

5.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 0.33 h / 20 °C

5.2: 2 h / Heating / reflux

With hydrogenchloride; dimethylsulfide borane complex; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; water;