(E)-1-(trimethylsilyloxy)-1-methyl-2-(6-methylhept-5-en-2-ylidene)cyclohex-3-ene

Base Information

Chemical Name:(E)-1-(trimethylsilyloxy)-1-methyl-2-(6-methylhept-5-en-2-ylidene)cyclohex-3-ene
CAS No.:1186190-04-4
Molecular Formula:C₁₈H₃₂OSi
Molecular Weight:292.537
Hs Code.:

Synonyms:(E)-1-(trimethylsilyloxy)-1-methyl-2-(6-methylhept-5-en-2-ylidene)cyclohex-3-ene

Suppliers and Price of (E)-1-(trimethylsilyloxy)-1-methyl-2-(6-methylhept-5-en-2-ylidene)cyclohex-3-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(trimethylsilyloxy)-1-methyl-2-(6-methylhept-5-en-2-ylidene)cyclohex-3-ene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (E)-1-(trimethylsilyloxy)-1-methyl-2-(6-methylhept-5-en-2-ylidene)cyclohex-3-ene

There total 2 articles about (E)-1-(trimethylsilyloxy)-1-methyl-2-(6-methylhept-5-en-2-ylidene)cyclohex-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1186189-90-1
(E)-3-(trimethylsilyloxy)-3,7,11-trimethyldodeca-6,10-dien-1-yne

: 1186190-04-4
(E)-1-(trimethylsilyloxy)-1-methyl-2-(6-methylhept-5-en-2-ylidene)cyclohex-3-ene

: 1186190-05-5
(E)-1-(trimethylsilyloxy)-1-methyl-2-(2,6-dimethylhepta-1,5-dienyl)cyclopent-2-ene

: 4-(trimethylsilyloxy)-(1aRS,4RS,4aSR,7bRS)-1,1,4,7-tetramethyl-1a,2,3,4,4a,5,6,7b-octahydro-1H-cyclopropa[e]azulene

: 4-(trimethylsilyloxy)-(1aRS,4SR,4aRS,7bSR)-1,1,4,7-tetramethyl-1a,2,3,4,4a,5,6,7b-octahydro-1H-cyclopropa[e]azulene

Guidance literature:: (E)-3-(trimethylsilyloxy)-3,7,11-trimethyldodeca-6,10-dien-1-yne; With 1,3‐bis[2,6‐bis(propan‐2‐yl)phenyl]‐2‐[(phenylformonitrile)aurio]‐2,3‐dihydro‐1H‐imidazol‐2‐yl hexafluorostibane; In dichloromethane; at 23 ℃; for 3h; Inert atmosphere; Molecular sieve;

With triethylamine; In hexane; dichloromethane; Molecular sieve;
DOI:10.1002/anie.200902248

Reference yield:

: 1186189-90-1
(E)-3-(trimethylsilyloxy)-3,7,11-trimethyldodeca-6,10-dien-1-yne

: 1186190-04-4
(E)-1-(trimethylsilyloxy)-1-methyl-2-(6-methylhept-5-en-2-ylidene)cyclohex-3-ene

: 4-(trimethylsilyloxy)-(1aRS,4RS,4aSR,7bRS)-1,1,4,7-tetramethyl-1a,2,3,4,4a,5,6,7b-octahydro-1H-cyclopropa[e]azulene

: 4-(trimethylsilyloxy)-(1aRS,4SR,4aRS,7bSR)-1,1,4,7-tetramethyl-1a,2,3,4,4a,5,6,7b-octahydro-1H-cyclopropa[e]azulene

Guidance literature:: (E)-3-(trimethylsilyloxy)-3,7,11-trimethyldodeca-6,10-dien-1-yne; With [Pt(CH₂C₆H₄P(o-tol)2)(MeCN)2]SbF₆; In dichloromethane; at 23 ℃; for 0.25h; Inert atmosphere; Molecular sieve;

With triethylamine; In hexane; dichloromethane; Molecular sieve;
DOI:10.1002/anie.200902248