1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

Base Information

Chemical Name:1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide
CAS No.:1256776-41-6
Molecular Formula:C₂₁H₃₃N₃O₄
Molecular Weight:391.511
Hs Code.:

Synonyms:1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

Suppliers and Price of 1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

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Technology Process of 1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

There total 1 articles about 1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1256776-38-1
2-(4-methyl-2-(morpholine-4-carboxamido)pentanoylamino)-4-phenylbutanoic acid methyl ester

: 1256776-41-6
1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

Guidance literature:: With sodium tetrahydroborate; calcium chloride; In tetrahydrofuran; methanol; for 5h;
DOI:10.1021/jm1009567

Reference yield: 53.0%

: 1256776-41-6
1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

: 438044-70-3
1-((1-formyl-3-phenylpropylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

Guidance literature:: 1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.25h;

With triethylamine; In dichloromethane; at -78 - 0 ℃;
DOI:10.1021/jm1009567

Reference yield:

: 1256776-41-6
1-((1-hydroxy-4-phenylbutan-2-ylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

: 1256776-27-8
C₃₁H₄₅N₃O₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.25 h / -78 °C

1.2: -78 - 0 °C

2.1: ozone / dichloromethane; pentane / -78 - 0 °C

With oxalyl dichloride; ozone; dimethyl sulfoxide; In dichloromethane; pentane; 1.1: Swern oxidation / 1.2: Swern oxidation / 2.1: Griesbaum co-ozonolysis;
DOI:10.1021/jm1009567