dicyclohexyl[2,2-di(methoxycarbonyl)-4,6,7-triphenyl-5-indanyl]phosphine sulfide

Base Information

Chemical Name:dicyclohexyl[2,2-di(methoxycarbonyl)-4,6,7-triphenyl-5-indanyl]phosphine sulfide
CAS No.:943443-66-1
Molecular Formula:C₄₃H₄₇O₄PS
Molecular Weight:690.884
Hs Code.:

Synonyms:dicyclohexyl[2,2-di(methoxycarbonyl)-4,6,7-triphenyl-5-indanyl]phosphine sulfide

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Chemical Property of dicyclohexyl[2,2-di(methoxycarbonyl)-4,6,7-triphenyl-5-indanyl]phosphine sulfide

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Technology Process of dicyclohexyl[2,2-di(methoxycarbonyl)-4,6,7-triphenyl-5-indanyl]phosphine sulfide

There total 2 articles about dicyclohexyl[2,2-di(methoxycarbonyl)-4,6,7-triphenyl-5-indanyl]phosphine sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 103991-65-7
dicyclohexyl(phenylethynyl)phosphine sulfide

: 2,2-bis-(3-phenyl-prop-2-ynyl)-malonic acid dimethyl ester

: 943443-66-1
dicyclohexyl[2,2-di(methoxycarbonyl)-4,6,7-triphenyl-5-indanyl]phosphine sulfide

Guidance literature:: With silver tetrafluoroborate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; chloro(1,5-cyclooctadiene)rhodium(I) dimer; In dichloromethane; at 25 ℃; for 4h;
DOI:10.1021/ja071622o

Reference yield:

: 95813-10-8
2-(dicyclohexylphosphino)-1-phenylethyne

: 943443-66-1
dicyclohexyl[2,2-di(methoxycarbonyl)-4,6,7-triphenyl-5-indanyl]phosphine sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfur

2: 83 percent / rac-BINAP; AgBF₄ / [RhCl(cod)]2 / CH₂Cl₂ / 4 h / 25 °C

With silver tetrafluoroborate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sulfur; chloro(1,5-cyclooctadiene)rhodium(I) dimer; In dichloromethane;
DOI:10.1021/ja071622o