sulfamic acid 3-(4-fluoro-phenyl)-propyl ester

Base Information

• Chemical Name: sulfamic acid 3-(4-fluoro-phenyl)-propyl ester
• CAS No.: 723287-07-8
• Molecular Formula: C₉H₁₂FNO₃S
• Molecular Weight: 233.264
• Mol file: 723287-07-8.mol

Synonyms:sulfamic acid 3-(4-fluoro-phenyl)-propyl ester

Chemical Property of sulfamic acid 3-(4-fluoro-phenyl)-propyl ester

Chemical Property:

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Technology Process of sulfamic acid 3-(4-fluoro-phenyl)-propyl ester

There total 1 articles about sulfamic acid 3-(4-fluoro-phenyl)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-fluorophenyl)propan-1-ol (702-15-8) → sulfamic acid 3-(4-fluoro-phenyl)-propyl ester (723287-07-8)

Guidance literature:

DOI:10.1021/jo0358877

Reference yield: 81.0%

sulfamic acid 3-(4-fluoro-phenyl)-propyl ester (723287-07-8) → 4-(4-fluoro-phenyl)-[1,2,3]oxathiazinane 2,2-dioxide

Guidance literature:

With aluminum oxide; [bis(acetoxy)iodo]benzene; 4 A molecular sieve; carbonyl(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)ruthenium(II); In dichloromethane; at 40 ℃; for 2h;

DOI:10.1021/jo0358877

Reference yield:

sulfamic acid 3-(4-fluoro-phenyl)-propyl ester (723287-07-8) → (S)-4-(4-Fluoro-phenyl)-[1,2,3]oxathiazinane 2,2-dioxide + (R)-4-(4-Fluoro-phenyl)-[1,2,3]oxathiazinane 2,2-dioxide

Guidance literature:

With aluminum oxide; [bis(acetoxy)iodo]benzene; 4 A molecular sieve; chiral ruthenium porphyrine catalyst; In benzene; at 5 ℃; for 8h; Title compound not separated from byproducts;

DOI:10.1021/jo0358877

upstream raw materials:

3-(4-fluorophenyl)propan-1-ol