[5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophen-3-yl]phenylmethanone

Base Information

Chemical Name:[5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophen-3-yl]phenylmethanone
CAS No.:1018831-20-3
Molecular Formula:C₂₃H₁₉BrF₃NO₃S
Molecular Weight:526.374
Hs Code.:

Synonyms:[5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophen-3-yl]phenylmethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophen-3-yl]phenylmethanone

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Technology Process of [5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophen-3-yl]phenylmethanone

There total 1 articles about [5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophen-3-yl]phenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1018831-18-9
C₂₃H₂₀F₃NO₃S

: 1018831-20-3
[5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophen-3-yl]phenylmethanone

Guidance literature:: With N-Bromosuccinimide; acetic acid; In dichloromethane; at -18 - -16 ℃; for 0.5h;
DOI:10.1016/j.bmc.2007.10.065

Reference yield: 69.0%

: 1018831-20-3
[5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophen-3-yl]phenylmethanone

: 24067-17-2
4-nitrophenylboronic acid

: 1053172-36-3
C₂₉H₂₃F₃N₂O₅S

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 70 - 80 ℃; for 24h;
DOI:10.1016/j.bmc.2007.10.065

Reference yield: 50.0%

: 1018831-20-3
[5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophen-3-yl]phenylmethanone

: 149104-90-5
4-acetylphenylboronic acid

: 1053172-23-8
C₃₁H₂₆F₃NO₄S

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 70 - 80 ℃; for 24h;
DOI:10.1016/j.bmc.2007.10.065