1,3-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-5-(bromomethyl)benzene

Base Information

Chemical Name:1,3-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-5-(bromomethyl)benzene
CAS No.:339531-07-6
Molecular Formula:C₆₅H₇₅BrO₆
Molecular Weight:1032.21
Hs Code.:

Synonyms:1,3-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-5-(bromomethyl)benzene

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Chemical Property of 1,3-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-5-(bromomethyl)benzene

Chemical Property:

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Technology Process of 1,3-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-5-(bromomethyl)benzene

There total 9 articles about 1,3-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-5-(bromomethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 339531-06-5
{3,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]phenyl}methanol

: 339531-07-6
1,3-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-5-(bromomethyl)benzene

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1002/1522-2675(20010228)84:2<296::AID-HLCA296>3.0.CO;2-X

Reference yield:

: 339531-03-2
5-(bromomethyl)-1,3-bis{[4-(tert-butyl)benzyl]oxy}benzene

: 339531-07-6
1,3-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-5-(bromomethyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / potassium carbonate; 18-crown-6 / acetone / 48 h / Heating

2: 85 percent / LiAlH₄ / tetrahydrofuran / 4 h / 20 °C

3: 95 percent / carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1021/ol062793l

Reference yield:

: 339531-02-1
(3,5-bis{[4-(tert-butyl)benzyl]oxy}phenyl)methanol

: 339531-07-6
1,3-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-5-(bromomethyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

2: 91 percent / potassium carbonate; 18-crown-6 / acetone / 48 h / Heating

3: 85 percent / LiAlH₄ / tetrahydrofuran / 4 h / 20 °C

4: 95 percent / carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1021/ol062793l