R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid

Base Information

Chemical Name:R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid
CAS No.:1443646-29-4
Molecular Formula:C₁₈H₂₄BN₃O₄
Molecular Weight:357.217
Hs Code.:

Synonyms:R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid

Suppliers and Price of R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid

There total 7 articles about R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84110-40-7
Dihydroxy-isobutyl-boran

: 1443646-22-7
C₂₈H₃₈BN₃O₄

: 1443646-29-4
R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid

Guidance literature:: With hydrogenchloride; In methanol; hexane; at 20 ℃; for 18h;
DOI:10.1016/j.ejmech.2013.03.032

Reference yield:

: 1443646-09-0
(4-phenylamino-2-oxo-2H-pyridin-1-yl)-acetic acid ethyl ester

: 1443646-29-4
R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; lithium hydroxide / ethanol / 4 h / 0 - 20 °C

2.1: benzotriazol-1-ol / dichloromethane / 0.33 h / -5 °C

2.2: 3 h / -15 - 20 °C

3.1: hydrogenchloride / methanol; hexane / 18 h / 20 °C

With hydrogenchloride; water; benzotriazol-1-ol; lithium hydroxide; In methanol; ethanol; hexane; dichloromethane;
DOI:10.1016/j.ejmech.2013.03.032

Reference yield:

: 1443646-15-8
(4-phenylamino-2-oxo-2H-pyridin-1-yl)-acetic acid

: 1443646-29-4
R-1-[2-(4-phenylamino-2-oxo-2H-pyridin-1-yl)acetamido]-3-methylbutylboronic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol / dichloromethane / 0.33 h / -5 °C

1.2: 3 h / -15 - 20 °C

2.1: hydrogenchloride / methanol; hexane / 18 h / 20 °C

With hydrogenchloride; benzotriazol-1-ol; In methanol; hexane; dichloromethane;
DOI:10.1016/j.ejmech.2013.03.032