meso-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol

Base Information

• Chemical Name: meso-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol
• CAS No.: 22210-57-7
• Molecular Formula: C₂₀H₂₆O₂
• Molecular Weight: 298.425

Synonyms:meso-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol

Chemical Property of meso-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol

Chemical Property:

Purity/Quality:

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Technology Process of meso-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol

There total 4 articles about meso-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

phenyl isopropyl ketone (611-70-1) → meso-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol (22210-57-7)

Guidance literature:

With tert-butyl isocyanide; titanium chloride; zinc; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1246/cl.1998.1107

Reference yield: 71.0%

phenyl isopropyl ketone (611-70-1) → meso-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol (22210-57-7) + dl-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol (22210-57-7,59214-60-7,66583-45-7,91361-10-3,22210-56-6)

Guidance literature:

phenyl isopropyl ketone; With iron(III)-acetylacetonate; phenyltriisopropoxytitanium(IV); In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; at 0 - 20 ℃; optical yield given as %de;

DOI:10.1246/cl.2011.492

Reference yield: 71.0%

phenyl isopropyl ketone (611-70-1) → meso-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol (22210-57-7) + dl-2,5-dimethyl-3,4-diphenyl-3,4-hexanediol (22210-57-7,59214-60-7,66583-45-7,91361-10-3,22210-56-6)

Guidance literature:

phenyl isopropyl ketone; With iron(III)-acetylacetonate; phenyltriisopropoxytitanium(IV); In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; at 0 - 20 ℃; optical yield given as %de;

DOI:10.1246/cl.2011.492

upstream raw materials:

phenyl isopropyl ketone

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