2,6-dimethyl-4-(4-nitrophenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid [3-(4,4-diphenylpiperidine-1-yl)-propyl] ester methyl ester

Base Information

Chemical Name:2,6-dimethyl-4-(4-nitrophenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid [3-(4,4-diphenylpiperidine-1-yl)-propyl] ester methyl ester
CAS No.:157066-79-0
Molecular Formula:C₃₆H₃₉N₃O₆
Molecular Weight:609.722
Hs Code.:

Synonyms:2,6-dimethyl-4-(4-nitrophenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid [3-(4,4-diphenylpiperidine-1-yl)-propyl] ester methyl ester

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Chemical Property of 2,6-dimethyl-4-(4-nitrophenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid [3-(4,4-diphenylpiperidine-1-yl)-propyl] ester methyl ester

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Technology Process of 2,6-dimethyl-4-(4-nitrophenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid [3-(4,4-diphenylpiperidine-1-yl)-propyl] ester methyl ester

There total 6 articles about 2,6-dimethyl-4-(4-nitrophenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid [3-(4,4-diphenylpiperidine-1-yl)-propyl] ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 555-16-8
4-nitrobenzaldehdye

: 116395-62-1
acetoacetic acid 3-(4,4-diphenylpiperidin-1-yl)propyl ester

: 14205-39-1
methyl 3-aminocrotonate

: 157066-79-0
2,6-dimethyl-4-(4-nitrophenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid [3-(4,4-diphenylpiperidine-1-yl)-propyl] ester methyl ester

Guidance literature:: In isopropyl alcohol;
DOI:10.1021/jm00010a001

Reference yield:

: 40064-34-4
piperidine-4,4-diol hydrochloride

: 157066-79-0
2,6-dimethyl-4-(4-nitrophenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid [3-(4,4-diphenylpiperidine-1-yl)-propyl] ester methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / AlCl₃

2: 76 percent / K₂CO₃ / dioxane

3: 95 percent / toluene

4: 51 percent / propan-2-ol

With aluminium trichloride; potassium carbonate; In 1,4-dioxane; isopropyl alcohol; toluene;
DOI:10.1021/jm00010a001

Reference yield:

: 4,4-Diphenylpiperidine hydrochloride

: 157066-79-0
2,6-dimethyl-4-(4-nitrophenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid [3-(4,4-diphenylpiperidine-1-yl)-propyl] ester methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / K₂CO₃ / dioxane

2: 95 percent / toluene

3: 51 percent / propan-2-ol

With potassium carbonate; In 1,4-dioxane; isopropyl alcohol; toluene;
DOI:10.1021/jm00010a001