(2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane

Base Information

Chemical Name:(2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane
CAS No.:233599-74-1
Molecular Formula:C₂₄H₄₂O₃Si
Molecular Weight:406.681
Hs Code.:

(2R,4R,4R,5R)-1-Benzyloxy-3,5-<<bis(1,1-dimethylethyl)silylene>dioxy>-2,4-dimethylheptane

Synonyms:(2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane

Suppliers and Price of (2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane

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Technology Process of (2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane

There total 3 articles about (2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 85272-31-7
di-tert-butylsilyl bis(trifluoromethanesulfonate)

: 198129-30-5
(2R,4R,4R,5R)-1-Benzyloxy-2,4-dimethylheptane-3,5-diol

: 233599-74-1
(2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 20 ℃; for 21h;
DOI:10.1039/a809818b

Reference yield:

: 116652-75-6
(R)-1-(benzyloxy)-2-methylpentan-3-one

: 233599-74-1
(2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane

Guidance literature:: Multi-step reaction with 3 steps

2: 91 percent / Me₄NBH(OAc)3, AcOH / acetonitrile / 1.) -25 deg C, 30 min, 2.) cooling, 13 h

3: 83 percent / 2,6-lutidine / CH₂Cl₂ / 21 h / 20 °C

With 2,6-dimethylpyridine; acetic acid; tetramethylammonium triacetoxyborohydride; In dichloromethane; acetonitrile;
DOI:10.1039/a809818b

Reference yield:

: 198129-29-2
(2R,4R,5R)-1-(Benzyloxy)-5-hydroxy-2,4-dimethylheptan-3-one

: 233599-74-1
(2R,4R,4R,5R)-1-Benzyloxy-3,5-<dioxy>-2,4-dimethylheptane

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Me₄NBH(OAc)3, AcOH / acetonitrile / 1.) -25 deg C, 30 min, 2.) cooling, 13 h

2: 83 percent / 2,6-lutidine / CH₂Cl₂ / 21 h / 20 °C

With 2,6-dimethylpyridine; acetic acid; tetramethylammonium triacetoxyborohydride; In dichloromethane; acetonitrile;
DOI:10.1039/a809818b