5'-[3,5-bis-(4-bromo-benzyl)-1H-pyrrol-2-ylmethylene]-4'-methoxy-1H,5'H-[2,2']bipyrrolyl

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Chemical Name:5'-[3,5-bis-(4-bromo-benzyl)-1H-pyrrol-2-ylmethylene]-4'-methoxy-1H,5'H-[2,2']bipyrrolyl
CAS No.:1314252-80-6
Molecular Formula:C₂₈H₂₃Br₂N₃O
Molecular Weight:577.318
Hs Code.:

Synonyms:5'-[3,5-bis-(4-bromo-benzyl)-1H-pyrrol-2-ylmethylene]-4'-methoxy-1H,5'H-[2,2']bipyrrolyl

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Chemical Property of 5'-[3,5-bis-(4-bromo-benzyl)-1H-pyrrol-2-ylmethylene]-4'-methoxy-1H,5'H-[2,2']bipyrrolyl

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Technology Process of 5'-[3,5-bis-(4-bromo-benzyl)-1H-pyrrol-2-ylmethylene]-4'-methoxy-1H,5'H-[2,2']bipyrrolyl

There total 4 articles about 5'-[3,5-bis-(4-bromo-benzyl)-1H-pyrrol-2-ylmethylene]-4'-methoxy-1H,5'H-[2,2']bipyrrolyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1314253-70-7
C₁₈H₁₅Br₂N

: 10476-41-2
4-methoxy-2,2'-bipyrrole-5-carboxaldehyde

: 1314252-80-6
5'-[3,5-bis-(4-bromo-benzyl)-1H-pyrrol-2-ylmethylene]-4'-methoxy-1H,5'H-[2,2']bipyrrolyl

Guidance literature:: With hydrogenchloride; In methanol; at 25 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jm200543y

Reference yield:

: 803712-71-2
N-((5-bromo-3-methoxy-2H-pyrrol-2-ylidene)-methyl)-N-ethylethanamine

: 1314252-80-6
5'-[3,5-bis-(4-bromo-benzyl)-1H-pyrrol-2-ylmethylene]-4'-methoxy-1H,5'H-[2,2']bipyrrolyl

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium diacetate; triphenylphosphine / 1,4-dioxane; water; toluene / 70 °C / Inert atmosphere

1.2: 3 h / 100 °C / Inert atmosphere

2.1: hydrogenchloride; water / pH 7 / Inert atmosphere

3.1: hydrogenchloride / methanol / 5 h / 25 °C / Inert atmosphere

With hydrogenchloride; water; palladium diacetate; triphenylphosphine; In 1,4-dioxane; methanol; water; toluene;
DOI:10.1021/jm200543y

Reference yield:

: C₁₄H₁₆N₂O₄

: 1314252-80-6
5'-[3,5-bis-(4-bromo-benzyl)-1H-pyrrol-2-ylmethylene]-4'-methoxy-1H,5'H-[2,2']bipyrrolyl

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / pH 7 / Inert atmosphere

2: hydrogenchloride / methanol / 5 h / 25 °C / Inert atmosphere

With hydrogenchloride; water; In methanol;
DOI:10.1021/jm200543y