Technology Process of C32H44O4Si
There total 7 articles about C32H44O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C32H44O3Si;
With
lithium diisopropyl amide;
In
tetrahydrofuran;
at -78 ℃;
for 0.5h;
With
2-[(4-methylphenyl)sulfonyl]-3-phenyl-oxaziridine;
at -78 - 20 ℃;
for 18.5h;
DOI:10.1016/j.tetlet.2013.07.137
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C
2.1: manganese(IV) oxide / dichloromethane / 20 h / 20 °C
3.1: 1H-imidazole / dichloromethane / 16 h / 0 °C
4.1: L-proline / tetrahydrofuran / 3 h / 65 °C / Inert atmosphere
5.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 1.5 h / 20 °C
6.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
6.2: 18.5 h / -78 - 20 °C
With
1H-imidazole; manganese(IV) oxide; 5%-palladium/activated carbon; tetrabutyl ammonium fluoride; hydrogen; L-proline; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/j.tetlet.2013.07.137
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: L-proline / tetrahydrofuran / 3 h / 65 °C / Inert atmosphere
2.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 1.5 h / 20 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
3.2: 18.5 h / -78 - 20 °C
With
5%-palladium/activated carbon; hydrogen; L-proline; lithium diisopropyl amide;
In
tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.tetlet.2013.07.137
