(S)-3-(((benzyloxy)carbonyl)amino)-4-((tert-butyldiphenylsilyl)oxy)butanoic acid

Base Information

Chemical Name:(S)-3-(((benzyloxy)carbonyl)amino)-4-((tert-butyldiphenylsilyl)oxy)butanoic acid
CAS No.:461009-54-1
Molecular Formula:C₂₈H₃₃NO₅Si
Molecular Weight:491.659
Hs Code.:

Synonyms:(S)-3-(((benzyloxy)carbonyl)amino)-4-((tert-butyldiphenylsilyl)oxy)butanoic acid

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Chemical Property of (S)-3-(((benzyloxy)carbonyl)amino)-4-((tert-butyldiphenylsilyl)oxy)butanoic acid

Chemical Property:

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Technology Process of (S)-3-(((benzyloxy)carbonyl)amino)-4-((tert-butyldiphenylsilyl)oxy)butanoic acid

There total 5 articles about (S)-3-(((benzyloxy)carbonyl)amino)-4-((tert-butyldiphenylsilyl)oxy)butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94664-82-1
(3S)-3-benzyloxycarbonylamino-4-hydroxybutanoic acid

: 58479-61-1
tert-butylchlorodiphenylsilane

: 461009-54-1
(S)-3-(((benzyloxy)carbonyl)amino)-4-((tert-butyldiphenylsilyl)oxy)butanoic acid

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 15h;

Reference yield:

: C₃₂H₄₁NO₅Si

: 461009-54-1
(S)-3-(((benzyloxy)carbonyl)amino)-4-((tert-butyldiphenylsilyl)oxy)butanoic acid

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1039/c7ob01403a

Reference yield:

: 146398-02-9
tert-butyl (S)-3-benzyloxycarbonylamino-4-hydroxybutyrate

: 461009-54-1
(S)-3-(((benzyloxy)carbonyl)amino)-4-((tert-butyldiphenylsilyl)oxy)butanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0.5 h / 20 °C

With 1H-imidazole; dmap; triethylamine; In dichloromethane;
DOI:10.1039/c7ob01403a