4-(trans-4-butylcyclohexyl)phenylmethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:4-(trans-4-butylcyclohexyl)phenylmethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
CAS No.:1616345-43-7
Molecular Formula:C₃₁H₄₄O₁₀
Molecular Weight:576.684
Hs Code.:

Synonyms:4-(trans-4-butylcyclohexyl)phenylmethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Chemical Property of 4-(trans-4-butylcyclohexyl)phenylmethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Technology Process of 4-(trans-4-butylcyclohexyl)phenylmethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

There total 4 articles about 4-(trans-4-butylcyclohexyl)phenylmethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616345-38-0
ethyl 4-(trans-4-butylcyclohexyl)benzoate

: 1616345-43-7
4-(trans-4-butylcyclohexyl)phenylmethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2: silver trifluoromethanesulfonate / dichloromethane

With lithium aluminium tetrahydride; silver trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; 2: |Koenigs-Knorr Glycosidation;
DOI:10.1016/j.carres.2014.04.007

Reference yield:

: 83626-35-1
p-(4-trans-butylcyclohexyl)benzoic acid

: 1616345-43-7
4-(trans-4-butylcyclohexyl)phenylmethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 16 h / 70 °C / Molecular sieve; Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3: silver trifluoromethanesulfonate / dichloromethane

With lithium aluminium tetrahydride; sulfuric acid; silver trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; 3: |Koenigs-Knorr Glycosidation;
DOI:10.1016/j.carres.2014.04.007

Reference yield:

: 3947-62-4,6207-76-7,19235-21-3,22554-70-7,22860-22-6,47339-09-3,57884-82-9,62057-79-8,70191-05-8,109525-54-4,140147-37-1,10343-06-3
2,3,4,5-tetra-O-acetyl-D-glucopyranose

: 1616345-43-7
4-(trans-4-butylcyclohexyl)phenylmethyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 5 h / -10 - -5 °C / Inert atmosphere

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 9 h / -5 °C / Molecular sieve; Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1016/j.carres.2014.04.007