Technology Process of C65H76O31
There total 6 articles about C65H76O31 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
dichloromethane;
at 20 ℃;
for 24h;
DOI:10.1071/CH12013
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: water; toluene-4-sulfonic acid / ethanol / 0.5 h / 50 °C
2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 14 h / 0 °C
3.1: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h
4.1: potassium hydrogencarbonate / acetone / 2 h
4.2: 48 h / 70 °C
5.1: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h
6.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C
With
triethylsilane; dmap; water; potassium hydrogencarbonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
ethanol; dichloromethane; acetone;
DOI:10.1071/CH12013
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 14 h / 0 °C
2.1: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h
3.1: potassium hydrogencarbonate / acetone / 2 h
3.2: 48 h / 70 °C
4.1: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h
5.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C
With
triethylsilane; dmap; potassium hydrogencarbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
dichloromethane; acetone;
DOI:10.1071/CH12013
