C₃₂H₃₈O₉S

Base Information

Chemical Name:C₃₂H₃₈O₉S
CAS No.:1257239-79-4
Molecular Formula:C₃₂H₃₈O₉S
Molecular Weight:598.714
Hs Code.:

C<sub>32</sub>H<sub>38</sub>O<sub>9</sub>S

Synonyms:C₃₂H₃₈O₉S

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Chemical Property of C₃₂H₃₈O₉S

Chemical Property:

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Technology Process of C₃₂H₃₈O₉S

There total 11 articles about C₃₂H₃₈O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1257239-78-3
C₂₈H₃₂O₈S

: 79-30-1
isobutyryl chloride

: 1257239-79-4
C₃₂H₃₈O₉S

Guidance literature:: With triethylamine; dmap; In dichloromethane; at 0 - 20 ℃; for 16h;

Reference yield:

: 620630-82-2
1,2 5,6-O-di(isopropylidene)-α-D-allofuranose

: 1257239-79-4
C₃₂H₃₈O₉S

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / Cooling with ice

2.1: water; acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane; water / 1.67 h

4.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 0.5 h / -78 °C

7.1: toluene; diethyl ether / 4 h / -78 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C

9.1: pyridine / 22 h / 0 - 20 °C

10.1: triethylamine / dmap / dichloromethane / 16 h / 0 - 20 °C

With pyridine; sodium periodate; oxalyl dichloride; tetrabutyl ammonium fluoride; water; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; dmap; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 939-26-4
2-bromomethylnaphthyl bromide

: 1257239-79-4
C₃₂H₃₈O₉S

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / Cooling with ice

2.1: water; acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane; water / 1.67 h

4.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 0.5 h / -78 °C

7.1: toluene; diethyl ether / 4 h / -78 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C

9.1: pyridine / 22 h / 0 - 20 °C

10.1: triethylamine / dmap / dichloromethane / 16 h / 0 - 20 °C

With pyridine; sodium periodate; oxalyl dichloride; tetrabutyl ammonium fluoride; water; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; dmap; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil;