Methyl (2R,3R,Z)-2-phenyl-3-{N-[13′′-(pyridin-3′′′-yl)tridecyl]amino}-16-(pyridin-3′-yl)hexadec-13-enoate

Base Information

Chemical Name:Methyl (2R,3R,Z)-2-phenyl-3-{N-[13′′-(pyridin-3′′′-yl)tridecyl]amino}-16-(pyridin-3′-yl)hexadec-13-enoate
CAS No.:1569300-04-4
Molecular Formula:C₄₆H₆₉N₃O₂
Molecular Weight:696.073
Hs Code.:

Synonyms:Methyl (2R,3R,Z)-2-phenyl-3-{N-[13′′-(pyridin-3′′′-yl)tridecyl]amino}-16-(pyridin-3′-yl)hexadec-13-enoate

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Chemical Property of Methyl (2R,3R,Z)-2-phenyl-3-{N-[13′′-(pyridin-3′′′-yl)tridecyl]amino}-16-(pyridin-3′-yl)hexadec-13-enoate

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Technology Process of Methyl (2R,3R,Z)-2-phenyl-3-{N-[13′′-(pyridin-3′′′-yl)tridecyl]amino}-16-(pyridin-3′-yl)hexadec-13-enoate

There total 11 articles about Methyl (2R,3R,Z)-2-phenyl-3-{N-[13′′-(pyridin-3′′′-yl)tridecyl]amino}-16-(pyridin-3′-yl)hexadec-13-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₆H₆₇N₃O₂

: 1569300-04-4
Methyl (2R,3R,Z)-2-phenyl-3-{N-[13′′-(pyridin-3′′′-yl)tridecyl]amino}-16-(pyridin-3′-yl)hexadec-13-enoate

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 16h;
DOI:10.1021/ol500096r

Reference yield:

: 1569300-01-1
methyl (2R,3R,R_S,Z)-2-phenyl-3-(N-tert-butylsulfinamido)-16-(pyridin-3′-yl)hexadec-13-enoate

: 1569300-04-4
Methyl (2R,3R,Z)-2-phenyl-3-{N-[13′′-(pyridin-3′′′-yl)tridecyl]amino}-16-(pyridin-3′-yl)hexadec-13-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol / 2 h / 20 °C

2: 1,2-dichloro-ethane / 0.08 h / 20 °C

3: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 16 h / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; acetic acid; In methanol; 1,2-dichloro-ethane;
DOI:10.1021/ol500096r

Reference yield:

: 133835-21-9
(Z)-14-(pyridin-3'-yl)tetradec-11-en-1-ol

: 1569300-04-4
Methyl (2R,3R,Z)-2-phenyl-3-{N-[13′′-(pyridin-3′′′-yl)tridecyl]amino}-16-(pyridin-3′-yl)hexadec-13-enoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C

2.1: pyridinium p-toluenesulfonate; magnesium sulfate / dichloromethane / 16 h / 20 °C

3.1: methylmagnesium bromide; magnesium bromide / diethyl ether; tetrahydrofuran / 1 h / -78 °C

3.2: 6 h / -78 °C

4.1: hydrogenchloride / methanol / 2 h / 20 °C

5.1: 1,2-dichloro-ethane / 0.08 h / 20 °C

6.1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 16 h / 20 °C

With hydrogenchloride; methylmagnesium bromide; pyridinium p-toluenesulfonate; sodium tris(acetoxy)borohydride; magnesium sulfate; acetic acid; magnesium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1021/ol500096r