Technology Process of C29H41NO9
There total 4 articles about C29H41NO9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
ethanol;
at 20 ℃;
for 4h;
DOI:10.1016/j.bmc.2013.03.013
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trifluoroacetic anhydride; 18-crown-6 ether; tetrabutylammonium nitrate / dichloromethane / 1 h / 20 °C
2: nickel chloride monohydrate; sodium tetrahydroborate / methanol; tetrahydrofuran / 4 °C
3: triethylamine / dichloromethane / 4 h / 20 °C
4: palladium on activated charcoal; hydrogen / ethanol / 4 h / 20 °C
With
sodium tetrahydroborate; 18-crown-6 ether; nickel chloride monohydrate; palladium on activated charcoal; hydrogen; tetrabutylammonium nitrate; triethylamine; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmc.2013.03.013
- Guidance literature:
-
Multi-step reaction with 3 steps
1: nickel chloride monohydrate; sodium tetrahydroborate / methanol; tetrahydrofuran / 4 °C
2: triethylamine / dichloromethane / 4 h / 20 °C
3: palladium on activated charcoal; hydrogen / ethanol / 4 h / 20 °C
With
sodium tetrahydroborate; nickel chloride monohydrate; palladium on activated charcoal; hydrogen; triethylamine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmc.2013.03.013
