Technology Process of 2-amino-2-methyl-6-heptenoic acid amide
There total 1 articles about 2-amino-2-methyl-6-heptenoic acid amide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: aq. NH4OH5; AcOH / methanol / 24 h / 20 °C
2.1: PhCHO / aq. NaOH; ethanol / 4 h / 20 °C
2.2: 13 g / aq. HCl / 4 h / 20 °C
With
benzaldehyde; acetic acid;
In
methanol; sodium hydroxide; ethanol;
1.1: Strecker synthesis;
DOI:10.1002/adsc.200600446
- Guidance literature:
-
With
amidase from Mycobacterium neoaurum ATCC 25795 (whole cells);
In
water;
at 37 ℃;
for 18h;
pH=8.3;
Enzymatic reaction;
DOI:10.1002/adsc.200600446
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 42 percent / amidase from Mycobacterium neoaurum ATCC 25795 (whole cells) / H2O / 18 h / 37 °C / pH 8.3 / Enzymatic reaction
2: SOCl2 / methanol / Heating
3: Et3N / CH2Cl2 / 20 °C
4: 50 percent / (1,3-dimesitylimidazolidin-2-yl)(PCy3)benzylidene-RuCl2 / toluene / 17 h / 95 °C
With
thionyl chloride; triethylamine;
(1,3-dimesitylimidazolidin-2-yl)(PCy3)benzylidene-RuCl2;
In
methanol; dichloromethane; water; toluene;
DOI:10.1002/adsc.200600446
