3,6-bis(acetylamino)-N-(3,4,5-tris((2S)-2-(2-(2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy)-ethoxy)-propoxy)-phenyl)-phthalimide

Base Information

Chemical Name:3,6-bis(acetylamino)-N-(3,4,5-tris((2S)-2-(2-(2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy)-ethoxy)-propoxy)-phenyl)-phthalimide
CAS No.:878375-75-8
Molecular Formula:C₅₄H₈₇N₃O₂₂
Molecular Weight:1130.29
Hs Code.:

Synonyms:3,6-bis(acetylamino)-N-(3,4,5-tris((2S)-2-(2-(2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy)-ethoxy)-propoxy)-phenyl)-phthalimide

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Chemical Property of 3,6-bis(acetylamino)-N-(3,4,5-tris((2S)-2-(2-(2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy)-ethoxy)-propoxy)-phenyl)-phthalimide

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Technology Process of 3,6-bis(acetylamino)-N-(3,4,5-tris((2S)-2-(2-(2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy)-ethoxy)-propoxy)-phenyl)-phthalimide

There total 4 articles about 3,6-bis(acetylamino)-N-(3,4,5-tris((2S)-2-(2-(2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy)-ethoxy)-propoxy)-phenyl)-phthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 878375-71-4
3,4,5-tris[(2S)-2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)propoxy]aniline

: 497147-09-8
3,6-bis(acetylamino)phthalic anhydride

: 878375-75-8
3,6-bis(acetylamino)-N-(3,4,5-tris((2S)-2-(2-(2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy)-ethoxy)-propoxy)-phenyl)-phthalimide

Guidance literature:: In 1,4-dioxane; for 17h; Heating;
DOI:10.1021/ol0524757 DOI:10.1002/chem.200600476

Reference yield:

: 911838-30-7
3,4,5-Tris-[(S)-2-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-propoxy]-benzoyl chloride

: 878375-75-8
3,6-bis(acetylamino)-N-(3,4,5-tris((2S)-2-(2-(2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy)-ethoxy)-propoxy)-phenyl)-phthalimide

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / sodium azide / tetrahydrofuran; H₂O / 1 h / 5 °C

2: 100 percent / dioxane / 4 h / Heating

3: 97 percent / aq. potassium hydroxide / dioxane / 0.5 h / 90 °C

4: 90 percent / dioxane / 17 h / Heating

With potassium hydroxide; sodium azide; In tetrahydrofuran; 1,4-dioxane; water; 2: Curtius rearrangement;
DOI:10.1002/chem.200600476

Reference yield:

: 911838-32-9
5-isocyanato-1,2,3-tris[(2S)-2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)propoxy]benzene

: 878375-75-8
3,6-bis(acetylamino)-N-(3,4,5-tris((2S)-2-(2-(2-(2-(2-methoxyethoxy)-ethoxy)-ethoxy)-ethoxy)-propoxy)-phenyl)-phthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / aq. potassium hydroxide / dioxane / 0.5 h / 90 °C

2: 90 percent / dioxane / 17 h / Heating

With potassium hydroxide; In 1,4-dioxane;
DOI:10.1002/chem.200600476