Acetic acid 3-acetoxy-2-(2,4-dinitro-phenyl-NNO-azoxy)-2-nitro-propyl ester

Base Information

Chemical Name:Acetic acid 3-acetoxy-2-(2,4-dinitro-phenyl-NNO-azoxy)-2-nitro-propyl ester
CAS No.:147459-78-7
Molecular Formula:C₁₃H₁₃N₅O₁₁
Molecular Weight:415.273
Hs Code.:

Synonyms:Acetic acid 3-acetoxy-2-(2,4-dinitro-phenyl-NNO-azoxy)-2-nitro-propyl ester

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Chemical Property of Acetic acid 3-acetoxy-2-(2,4-dinitro-phenyl-NNO-azoxy)-2-nitro-propyl ester

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Technology Process of Acetic acid 3-acetoxy-2-(2,4-dinitro-phenyl-NNO-azoxy)-2-nitro-propyl ester

There total 4 articles about Acetic acid 3-acetoxy-2-(2,4-dinitro-phenyl-NNO-azoxy)-2-nitro-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 147459-75-4
1,3-diacetoxy-2-nitro-(2,4-dinitrophenylazo)propane

: 147459-78-7
Acetic acid 3-acetoxy-2-(2,4-dinitro-phenyl-NNO-azoxy)-2-nitro-propyl ester

Guidance literature:: With dihydrogen peroxide; trifluoroacetic anhydride; In dichloromethane; for 3h; Heating;
DOI:10.1007/BF00863827

Reference yield:

: 54420-10-9
α,α-diacetoxyacetone 2,4-dinitrophenylhydrazone

: 147459-78-7
Acetic acid 3-acetoxy-2-(2,4-dinitro-phenyl-NNO-azoxy)-2-nitro-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / N₂O₄ / CH₂Cl₂ / 0.5 h / 20 °C

2: 37 percent / 88percent H₂O₂, trifluoroacetic anhydride / CH₂Cl₂ / 3 h / Heating

With dihydrogen peroxide; dinitrogen tetraoxide; trifluoroacetic anhydride; In dichloromethane;
DOI:10.1007/BF00863827

Reference yield:

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 147459-78-7
Acetic acid 3-acetoxy-2-(2,4-dinitro-phenyl-NNO-azoxy)-2-nitro-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / ethyl acetate / 0.5 h / Heating

2: 65 percent / 18-crown-6 / CHCl₃ / 2 h / Heating

3: 87 percent / N₂O₄ / CH₂Cl₂ / 0.5 h / 20 °C

4: 37 percent / 88percent H₂O₂, trifluoroacetic anhydride / CH₂Cl₂ / 3 h / Heating

With 18-crown-6 ether; dihydrogen peroxide; dinitrogen tetraoxide; trifluoroacetic anhydride; In dichloromethane; chloroform; ethyl acetate;
DOI:10.1007/BF00863827