3-methyl-4-nitro-5-<2-(3,5-dimethoxy-4-hydroxyphenyl)ethenyl>isoxazole

Base Information

• Chemical Name: 3-methyl-4-nitro-5-<2-(3,5-dimethoxy-4-hydroxyphenyl)ethenyl>isoxazole
• CAS No.: 85364-71-2
• Molecular Formula: C₁₄H₁₄N₂O₆
• Molecular Weight: 306.275
• Mol file: 85364-71-2.mol

Synonyms:3-methyl-4-nitro-5-<2-(3,5-dimethoxy-4-hydroxyphenyl)ethenyl>isoxazole

Chemical Property of 3-methyl-4-nitro-5-<2-(3,5-dimethoxy-4-hydroxyphenyl)ethenyl>isoxazole

Chemical Property:

Purity/Quality:

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Technology Process of 3-methyl-4-nitro-5-<2-(3,5-dimethoxy-4-hydroxyphenyl)ethenyl>isoxazole

There total 1 articles about 3-methyl-4-nitro-5-<2-(3,5-dimethoxy-4-hydroxyphenyl)ethenyl>isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.6%

3,5-dimethyl-4-nitroisoxazole (1123-49-5) + syringic aldehyde (134-96-3) → 3-methyl-4-nitro-5-<2-(3,5-dimethoxy-4-hydroxyphenyl)ethenyl>isoxazole (85364-71-2)

Guidance literature:

With piperidine;

Reference yield: 72.9%

3-methyl-4-nitro-5-<2-(3,5-dimethoxy-4-hydroxyphenyl)ethenyl>isoxazole (85364-71-2) → trans-3,5-dimethoxy-4-hydroxycinnamic acid (530-59-6,7362-37-0)

Guidance literature:

With sodium hydroxide; for 2h; Heating;

upstream raw materials:

3,5-dimethyl-4-nitroisoxazole

syringic aldehyde

Downstream raw materials:

trans-3,5-dimethoxy-4-hydroxycinnamic acid