trans-9-Styrylanthracene

Base Information

• Chemical Name: trans-9-Styrylanthracene
• CAS No.: 42196-97-4
• Molecular Formula: C22H16
• Molecular Weight: 280.369
• Hs Code.: 2902909090
• European Community (EC) Number: 255-705-8
• DSSTox Substance ID: DTXSID001297298
• Nikkaji Number: J278.356H,J915.254G
• Mol file: 42196-97-4.mol

Synonyms:trans-9-Styrylanthracene;1895-98-3;42196-97-4;(E)9-(2-Phenylvinyl)anthracene;9-[(E)-2-Phenylethenyl]anthracene;(9E)-Styrylanthracene;EINECS 255-705-8;Anthracene, 9-(2-phenylethenyl)-;9-styrylanthracene;9-styryl anthracene;(E)-9-styrylanthracene;9-[(E)-Styryl]anthracene;HCSGQHDONHRJCM-CCEZHUSRSA-N;DTXSID001297298;9-[(1E)-2-Phenylethenyl]anthracene;AKOS015909500;9-[(E)-2-Phenylethenyl]anthracene #;Z56756261

Chemical Property of trans-9-Styrylanthracene

Chemical Property:

• Vapor Pressure: 8.8E-09mmHg at 25°C
• Melting Point: 132 °C
• Boiling Point: 476.4°Cat760mmHg
• Flash Point: 236.5°C
• PSA: 0.00000
• Density: 1.163g/cm³
• LogP: 6.16340
• XLogP3: 6.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 280.125200510
• Heavy Atom Count: 22
• Complexity: 354

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C=CC2=C3C=CC=CC3=CC4=CC=CC=C42
• Isomeric SMILES: C1=CC=C(C=C1)/C=C/C2=C3C=CC=CC3=CC4=CC=CC=C42

Technology Process of trans-9-Styrylanthracene

There total 29 articles about trans-9-Styrylanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

9-anthracene aldehyde (642-31-9) → 9-trans-styryl-anthracene (42196-97-4)

Guidance literature:

With sodium hydroxide; cetyltrimethylammonim bromide; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1016/S0040-4039(00)74581-3

Reference yield: 98.0%

9-anthracene aldehyde (642-31-9) → 9-trans-styryl-anthracene (42196-97-4)

Guidance literature:

With crosslinked polymer-supported phosphonium salt of benzyl chloride; cetyltrimethylammonim bromide; In sodium hydroxide; dichloromethane; for 2h; Product distribution; Ambient temperature; without catalysts; other polymer supported phosphonium salt;

DOI:10.1016/S0040-4039(00)74581-3

Reference yield: 96.0%

bromobenzene (108-86-1,52753-63-6) + 9-vinylanthracene (2444-68-0) → 9-trans-styryl-anthracene (42196-97-4)

Guidance literature:

With {1,3-bis[2,6-bis(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}dichloro(pyridine)palladium; caesium carbonate; In neat (no solvent); at 100 ℃; for 12h;

DOI:10.1080/00397911.2021.1919711

upstream raw materials:

benzyl chloride

9-anthracene aldehyde

styrene

9-Bromoanthracene

Downstream raw materials:

12-(p-nitrobenzoyl)-1,3-dichloro-6-trans-styryl-11,12-dihydro-6,11<1',2'>-benzeno-6H-dibenz<1,4>oxazocine

C₄₄H₃₂

C₄₄H₃₂

C₄₄H₃₂