(S)-2-<4-<3-<<2-(3,4-dimethoxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4,5-dimethylimidazole

Base Information

Chemical Name:(S)-2-<4-<3-<<2-(3,4-dimethoxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4,5-dimethylimidazole
CAS No.:102152-17-0
Molecular Formula:C₂₄H₃₁N₃O₄
Molecular Weight:425.528
Hs Code.:

Synonyms:(S)-2-<4-<3-<<2-(3,4-dimethoxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4,5-dimethylimidazole

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Chemical Property of (S)-2-<4-<3-<<2-(3,4-dimethoxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4,5-dimethylimidazole

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Technology Process of (S)-2-<4-<3-<<2-(3,4-dimethoxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4,5-dimethylimidazole

There total 4 articles about (S)-2-<4-<3-<<2-(3,4-dimethoxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4,5-dimethylimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102151-42-8
2--4,5-dimethylimidazole

: 102152-17-0
(S)-2-<4-<3-<<2-(3,4-dimethoxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4,5-dimethylimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / ethanol / 95 h / 2585.7 Torr

2: 1.) NaH / 1.) DMF, 70 deg C, 15 min, 2.) DMF, 120 deg C, 18 h

3: H₂O, AcOH / 18 h / Ambient temperature

With water; hydrogen; sodium hydride; acetic acid; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00156a028

Reference yield:

: (S)-3-[2-(3,4-Dimethoxy-phenyl)-ethyl]-5-[4-(4,5-dimethyl-1H-imidazol-2-yl)-phenoxymethyl]-2-phenyl-oxazolidine

: 102152-17-0
(S)-2-<4-<3-<<2-(3,4-dimethoxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4,5-dimethylimidazole

Guidance literature:: With water; acetic acid; for 18h; Yield given; Ambient temperature;
DOI:10.1021/jm00156a028

Reference yield:

: 85613-47-4,85613-59-8,91944-23-9
(S)-2-phenyl-3-<2-(3,4-dimethoxyphenyl)ethyl>-5-(hydroxymethyl)oxazolidine p-toluenesulfonate

: 102152-17-0
(S)-2-<4-<3-<<2-(3,4-dimethoxyphenyl)ethyl>amino>-2-hydroxypropoxy>phenyl>-4,5-dimethylimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 70 deg C, 15 min, 2.) DMF, 120 deg C, 18 h

2: H₂O, AcOH / 18 h / Ambient temperature

With water; sodium hydride; acetic acid;
DOI:10.1021/jm00156a028