(E)-2-(3-((3,5-di(pyrrolidine-1-carbonyl)phenyl)diazenyl)phenyl)isoindoline-1,3-dione

Base Information

• Chemical Name: (E)-2-(3-((3,5-di(pyrrolidine-1-carbonyl)phenyl)diazenyl)phenyl)isoindoline-1,3-dione
• CAS No.: 1579998-95-0
• Molecular Formula: C₃₀H₂₇N₅O₄
• Molecular Weight: 521.575

Synonyms:(E)-2-(3-((3,5-di(pyrrolidine-1-carbonyl)phenyl)diazenyl)phenyl)isoindoline-1,3-dione

Chemical Property of (E)-2-(3-((3,5-di(pyrrolidine-1-carbonyl)phenyl)diazenyl)phenyl)isoindoline-1,3-dione

Chemical Property:

Purity/Quality:

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Technology Process of (E)-2-(3-((3,5-di(pyrrolidine-1-carbonyl)phenyl)diazenyl)phenyl)isoindoline-1,3-dione

There total 5 articles about (E)-2-(3-((3,5-di(pyrrolidine-1-carbonyl)phenyl)diazenyl)phenyl)isoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-(3-aminophenyl)isoindoline-1,3-dione (32338-22-0) + C16H19N3O3 (1579998-94-9) → (E)-2-(3-((3,5-di(pyrrolidine-1-carbonyl)phenyl)diazenyl)phenyl)isoindoline-1,3-dione (1579998-95-0)

Guidance literature:

With acetic acid; for 24h;

DOI:10.1021/ol500381c

Reference yield:

phthalic anhydride (85-44-9) → (E)-2-(3-((3,5-di(pyrrolidine-1-carbonyl)phenyl)diazenyl)phenyl)isoindoline-1,3-dione (1579998-95-0)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 8 h / Reflux; Dean-Stark

2: acetic acid / 24 h

With acetic acid; In toluene;

DOI:10.1021/ol500381c

Reference yield:

1,4-phenylenediamine (106-50-3) → (E)-2-(3-((3,5-di(pyrrolidine-1-carbonyl)phenyl)diazenyl)phenyl)isoindoline-1,3-dione (1579998-95-0)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 8 h / Reflux; Dean-Stark

2: acetic acid / 24 h

With acetic acid; In toluene;

DOI:10.1021/ol500381c

upstream raw materials:

2-(3-aminophenyl)isoindoline-1,3-dione

C₁₆H₁₉N₃O₃

5-aminoisophthalic acid

phthalic anhydride

Downstream raw materials:

(E)-(5-((3-aminophenyl)diazenyl)-1,3-phenylene)bis(pyrrolidin-1-ylmethanone)

(E)-1-(3,5-bis(trifluoromethyl)phenyl)-3-(3-((3,5-di(pyrrolidine-1-carbonyl)-phenyl)diazenyl)phenyl)thiourea

(Z)-1-(3,5-bis(trifluoromethyl)phenyl)-3-(3-((3,5-di(pyrrolidine-1-carbonyl)-phenyl)diazenyl)phenyl)thiourea

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