1-{3-[4-(tert-butyl)phenyl]-5-N,N-dimethylaminomethyl-(1,2,4-triazol-4-yl)}-3-methoxylbenzene

Base Information

Chemical Name:1-{3-[4-(tert-butyl)phenyl]-5-N,N-dimethylaminomethyl-(1,2,4-triazol-4-yl)}-3-methoxylbenzene
CAS No.:581814-71-3
Molecular Formula:C₂₂H₂₈N₄O
Molecular Weight:364.491
Hs Code.:

Synonyms:1-{3-[4-(tert-butyl)phenyl]-5-N,N-dimethylaminomethyl-(1,2,4-triazol-4-yl)}-3-methoxylbenzene

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Chemical Property of 1-{3-[4-(tert-butyl)phenyl]-5-N,N-dimethylaminomethyl-(1,2,4-triazol-4-yl)}-3-methoxylbenzene

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Technology Process of 1-{3-[4-(tert-butyl)phenyl]-5-N,N-dimethylaminomethyl-(1,2,4-triazol-4-yl)}-3-methoxylbenzene

There total 7 articles about 1-{3-[4-(tert-butyl)phenyl]-5-N,N-dimethylaminomethyl-(1,2,4-triazol-4-yl)}-3-methoxylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 581814-74-6
N³-[3-methoxyphenyl]-p-tert-butyl-benzamidrazone

: 33797-51-2
eschenmoser's salt

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 581814-71-3
1-{3-[4-(tert-butyl)phenyl]-5-N,N-dimethylaminomethyl-(1,2,4-triazol-4-yl)}-3-methoxylbenzene

Guidance literature:: at 80 ℃; for 5h;

Reference yield:

: 581814-73-5
4-tert-butyl-N-(3-methoxyphenyl)thiobenzamide

: 581814-71-3
1-{3-[4-(tert-butyl)phenyl]-5-N,N-dimethylaminomethyl-(1,2,4-triazol-4-yl)}-3-methoxylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: NH₂NH₂ / ethanol / 5 h / 20 °C

2: AcOH; DMF / 5 h

3: CH₂Cl₂ / 5 h

With acetic acid; N,N-dimethyl-formamide; hydrazine; In ethanol; dichloromethane;
DOI:10.1021/jm0601250

Reference yield:

: 129504-97-8
[4-(tert-butyl)phenyl]-N-(3-methoxyphenyl)carboxamide

: 581814-71-3
1-{3-[4-(tert-butyl)phenyl]-5-N,N-dimethylaminomethyl-(1,2,4-triazol-4-yl)}-3-methoxylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: Lawesson's reagent / CHCl₃ / 5 h / Heating

2: NH₂NH₂ / ethanol / 5 h / 20 °C

3: AcOH; DMF / 5 h

4: CH₂Cl₂ / 5 h

With Lawessons reagent; acetic acid; N,N-dimethyl-formamide; hydrazine; In ethanol; dichloromethane; chloroform;
DOI:10.1021/jm0601250