(2R)-2-[(1R,2S,3R,4R)-5-(benzyloxy)-1-hydroxy-3-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl]-4-pentenyl 4-methyl-1-benzenesulfonate

Base Information

Chemical Name:(2R)-2-[(1R,2S,3R,4R)-5-(benzyloxy)-1-hydroxy-3-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl]-4-pentenyl 4-methyl-1-benzenesulfonate
CAS No.:1201638-81-4
Molecular Formula:C₃₄H₄₄O₇S
Molecular Weight:596.785
Hs Code.:

Synonyms:(2R)-2-[(1R,2S,3R,4R)-5-(benzyloxy)-1-hydroxy-3-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl]-4-pentenyl 4-methyl-1-benzenesulfonate

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Chemical Property of (2R)-2-[(1R,2S,3R,4R)-5-(benzyloxy)-1-hydroxy-3-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl]-4-pentenyl 4-methyl-1-benzenesulfonate

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Technology Process of (2R)-2-[(1R,2S,3R,4R)-5-(benzyloxy)-1-hydroxy-3-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl]-4-pentenyl 4-methyl-1-benzenesulfonate

There total 1 articles about (2R)-2-[(1R,2S,3R,4R)-5-(benzyloxy)-1-hydroxy-3-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl]-4-pentenyl 4-methyl-1-benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1201638-80-3
(2R,3R,4S,5R,6R)-2-allyl-7-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-4,6-dimethylheptane-1,3-diol

: 98-59-9
p-toluenesulfonyl chloride

: 1201638-81-4
(2R)-2-[(1R,2S,3R,4R)-5-(benzyloxy)-1-hydroxy-3-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl]-4-pentenyl 4-methyl-1-benzenesulfonate

Guidance literature:: With triethylamine; at 0 - 25 ℃;
DOI:10.1016/j.tetasy.2009.08.021

Reference yield: 80.0%

: 1201638-81-4
(2R)-2-[(1R,2S,3R,4R)-5-(benzyloxy)-1-hydroxy-3-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl]-4-pentenyl 4-methyl-1-benzenesulfonate

: 1201638-82-5
(4S,5R,6S,7R,8R)-9-(benzyloxy)-7-[(4-methoxybenzyl)oxy]-4,6,8-trimethyl-1-nonen-5-ol

Guidance literature:: (2R)-2-[(1R,2S,3R,4R)-5-(benzyloxy)-1-hydroxy-3-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl]-4-pentenyl 4-methyl-1-benzenesulfonate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; Reflux;

With sodium sulfate; In tetrahydrofuran; diethyl ether; water; at 0 ℃; Saturated solution;
DOI:10.1016/j.tetasy.2009.08.021