3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate

Base Information

Chemical Name:3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate
CAS No.:1446518-33-7
Molecular Formula:C₁₀H₁₂O₄
Molecular Weight:196.203
Hs Code.:

Synonyms:3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate

Suppliers and Price of 3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate

There total 1 articles about 3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35718-08-2
propargyl chloroformate

: 815-57-6
3-Methyl-2,4-pentanedione

: 1446518-33-7
3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate

: 1446518-34-8
prop-2-ynyl 2-acetyl-2-methyl-3-oxobutanoate

Guidance literature:: 3-Methyl-2,4-pentanedione; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.166667h; Inert atmosphere;

propargyl chloroformate; In tetrahydrofuran; at 20 ℃; for 1h; Overall yield = 62 %; Overall yield = 209 mg; Inert atmosphere;
DOI:10.1021/ol401729m

Reference yield: 85.0%

: 874-23-7,125117-37-5
2-acetylcyclohexanone

: 1446518-33-7
3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate

: 3-(3-(1-acetyl-2-oxocyclohexyl)prop-1-en-2-yl)-3-methylpentane-2,4-dione

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; xantphos; In 1,4-dioxane; at 80 ℃; for 2h; Inert atmosphere; Sealed tube;
DOI:10.1055/s-0036-1591957

Reference yield: 73.0%

: 1134-87-8
3-benzyl-pentane-2,4-dione

: 1446518-33-7
3-methyl-4-oxopent-2-en-2-yl prop-2-ynyl carbonate

: 3,6-diacetyl-6-benzyl-3-methyl-4-methyleneoctane-2,7-dione

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; xantphos; In 1,4-dioxane; at 80 ℃; for 2h; Inert atmosphere; Sealed tube;
DOI:10.1055/s-0036-1591957