2-tert-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

Base Information

Chemical Name:2-tert-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester
CAS No.:936633-44-2
Molecular Formula:C₂₅H₂₉NO₄
Molecular Weight:407.51
Hs Code.:

2-<i>tert</i>-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

Synonyms:2-tert-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-tert-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

Chemical Property:

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Technology Process of 2-tert-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

There total 1 articles about 2-tert-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 690254-47-8
methyl (S)-2-(tert-butyloxycarbonyl)amino-1,2,3,4-tetrahydro-6-bromo-2-naphthalenecarboxylate

: 936633-44-2
2-tert-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

Guidance literature:: With 4 A molecular sieve; caesium carbonate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; tri-tert-butyl phosphine; In 1,4-dioxane; for 18h; Heating;
DOI:10.1021/jm0614073

Reference yield: 90.0%

: 936633-44-2
2-tert-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

: 936633-46-4
2-tert-butoxycarbonylamino-6-phenethyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃;
DOI:10.1021/jm0614073

Reference yield:

: 936633-44-2
2-tert-butoxycarbonylamino-6-styryl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

: 936633-48-6
2-tert-butoxycarbonylamino-6-phenethyl-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / hydrogen / Pd/C / ethyl acetate / 20 °C

2: 90 percent / lithium hydroxide monohydrate / tetrahydrofuran; methanol; H₂O / 20 °C

With lithium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; water; ethyl acetate;
DOI:10.1021/jm0614073