(rac)-4-(4-Chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal

Base Information

Chemical Name:(rac)-4-(4-Chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal
CAS No.:850565-90-1
Molecular Formula:C₁₄H₁₅ClF₄O₃
Molecular Weight:342.718
Hs Code.:

Synonyms:(rac)-4-(4-Chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal

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Chemical Property of (rac)-4-(4-Chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal

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Technology Process of (rac)-4-(4-Chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal

There total 1 articles about (rac)-4-(4-Chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 850565-89-8
rac-4-(4-chloro-3-fluoro-2-methoxyphenyl)-4-methyl-2-(trifluoromethyl)-2-hydroxy-pentanoic acid ethyl ester

: 850565-90-1
(rac)-4-(4-Chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal

Guidance literature:: rac-4-(4-chloro-3-fluoro-2-methoxyphenyl)-4-methyl-2-(trifluoromethyl)-2-hydroxy-pentanoic acid ethyl ester; With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 0.666667h;

With water; sodium hydrogencarbonate; In diethyl ether; at 0 - 20 ℃;

Reference yield: 80.0%

: 825654-64-6
7-fluoro-2-methylquinazolin-5-amine

: 850565-90-1
(rac)-4-(4-Chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal

: 850565-93-4
(rac.)-1,1,1-trifluoro-4-(4-chloro-3-fluoro-2-methoxyphenyl)-2-[(7-fluoro-2-methylquinazolin-5-yl)iminomethyl]-4-methylpentan-2-ol

Guidance literature:: With titanium(IV) isopropylate; rac-4-(4-chloro-3-fluoro-2-methoxyphenyl)-4-methyl-2-(trifluoromethyl)-2-hydroxy-pentanoic acid ethyl ester; In o-xylene; at 120 ℃; for 2h;

Reference yield: 30.4%

: 850565-90-1
(rac)-4-(4-Chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentanal

: 93117-08-9
5-aminoisoquinolin-1(2H)-one

: (rac.)-5-{[4-(4-chloro-3-fluoro-2-methoxyphenyl)-2-hydroxy-4-methyl-2-(trifluoromethyl)pentyliden]amino}-isoquinolin-1(2H)-one

Guidance literature:: With titanium(IV) isopropylate; rac-4-(4-chloro-3-fluoro-2-methoxyphenyl)-4-methyl-2-(trifluoromethyl)-2-hydroxy-pentanoic acid ethyl ester; In o-xylene; at 120 ℃; for 2h;