N₁,N₂-bis(tert-butoxycarbonyl)-N₁-(trans-cinnamyl)-S-methylisothiourea

Base Information

• Chemical Name: N₁,N₂-bis(tert-butoxycarbonyl)-N₁-(trans-cinnamyl)-S-methylisothiourea
• CAS No.: 1176817-71-2
• Molecular Formula: C₂₁H₃₀N₂O₄S
• Molecular Weight: 406.546

Synonyms:N₁,N₂-bis(tert-butoxycarbonyl)-N₁-(trans-cinnamyl)-S-methylisothiourea

Chemical Property of N₁,N₂-bis(tert-butoxycarbonyl)-N₁-(trans-cinnamyl)-S-methylisothiourea

Chemical Property:

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Technology Process of N₁,N₂-bis(tert-butoxycarbonyl)-N₁-(trans-cinnamyl)-S-methylisothiourea

There total 1 articles about N₁,N₂-bis(tert-butoxycarbonyl)-N₁-(trans-cinnamyl)-S-methylisothiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N,N'-bis-Boc-S-methyl-isothiourea (322474-21-5) + (2E)-3-phenyl-2-propen-1-ol (4407-36-7) → N1,N2-bis(tert-butoxycarbonyl)-N1-(trans-cinnamyl)-S-methylisothiourea (1176817-71-2)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; Reflux;

DOI:10.1021/jm900371z

Reference yield: 95.0%

N1,N2-bis(tert-butoxycarbonyl)-N1-(trans-cinnamyl)-S-methylisothiourea (1176817-71-2) + 5-tert-butoxycarbonylamino-1-aminopentane (51644-96-3) → (N1-5-aminopentyl)-N3-[(E)-3-phenyl-2-propenyl]-N1,N2,N3-tris(tert-butoxycarbonyl)-guanidine (1176817-86-9)

Guidance literature:

In tetrahydrofuran; at 50 ℃; for 18h; Heating;

DOI:10.1021/jm900371z

upstream raw materials:

N,N'-bis-Boc-S-methyl-isothiourea

(2E)-3-phenyl-2-propen-1-ol

Downstream raw materials:

(N₁-5-aminopentyl)-N₃-[(E)-3-phenyl-2-propenyl]-N₁,N₂,N₃-tris(tert-butoxycarbonyl)-guanidine

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