C₂₀H₁₅⁽²⁾HN₂O

Base Information

Chemical Name:C₂₀H₁₅⁽²⁾HN₂O
CAS No.:1310709-15-9
Molecular Formula:C₂₀H₁₆N₂O
Molecular Weight:301.352
Hs Code.:

C<sub>20</sub>H<sub>15</sub><sup>(2)</sup>HN<sub>2</sub>O

Synonyms:C₂₀H₁₅⁽²⁾HN₂O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₁₅⁽²⁾HN₂O

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Technology Process of C₂₀H₁₅⁽²⁾HN₂O

There total 4 articles about C₂₀H₁₅⁽²⁾HN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 1310709-13-7
3-deuterio-1-(pyridin-2-yl)-1H-indole

: 1310709-15-9
C₂₀H₁₅⁽²⁾HN₂O

Guidance literature:: With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 1-Adamantanecarboxylic acid; potassium carbonate; In m-xylene; at 120 ℃; for 22h; Inert atmosphere;
DOI:10.1021/ol2010648

Reference yield:

: 109-04-6
2-bromo-pyridine

: 1310709-15-9
C₂₀H₁₅⁽²⁾HN₂O

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; potassium phosphate; N,N`-dimethylethylenediamine / toluene / 24 h / 110 °C / Inert atmosphere

2: N-Bromosuccinimide / tetrahydrofuran / 0.25 h / 0 °C

3: water-d2; tert.-butyl lithium / tetrahydrofuran; pentane / 0.33 h / -78 °C

4: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 1-Adamantanecarboxylic acid; potassium carbonate / m-xylene / 22 h / 120 °C / Inert atmosphere

With potassium phosphate; N-Bromosuccinimide; copper(l) iodide; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 1-Adamantanecarboxylic acid; water-d2; tert.-butyl lithium; potassium carbonate; N,N`-dimethylethylenediamine; In tetrahydrofuran; m-xylene; toluene; pentane;
DOI:10.1021/ol2010648

Reference yield:

: 120-72-9
indole

: 1310709-15-9
C₂₀H₁₅⁽²⁾HN₂O

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; potassium phosphate; N,N`-dimethylethylenediamine / toluene / 24 h / 110 °C / Inert atmosphere

2: N-Bromosuccinimide / tetrahydrofuran / 0.25 h / 0 °C

3: water-d2; tert.-butyl lithium / tetrahydrofuran; pentane / 0.33 h / -78 °C

4: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 1-Adamantanecarboxylic acid; potassium carbonate / m-xylene / 22 h / 120 °C / Inert atmosphere

With potassium phosphate; N-Bromosuccinimide; copper(l) iodide; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 1-Adamantanecarboxylic acid; water-d2; tert.-butyl lithium; potassium carbonate; N,N`-dimethylethylenediamine; In tetrahydrofuran; m-xylene; toluene; pentane;
DOI:10.1021/ol2010648