N-[1(S)-ethoxycarbonyl-3-(1-benzyloxycarbonyl-4-piperidyl)propyl]-L-alanyl-L-proline benzylester

Base Information

Chemical Name:N-[1(S)-ethoxycarbonyl-3-(1-benzyloxycarbonyl-4-piperidyl)propyl]-L-alanyl-L-proline benzylester
CAS No.:120008-74-4
Molecular Formula:C₃₄H₄₅N₃O₇
Molecular Weight:607.747
Hs Code.:

Synonyms:N-[1(S)-ethoxycarbonyl-3-(1-benzyloxycarbonyl-4-piperidyl)propyl]-L-alanyl-L-proline benzylester

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Chemical Property of N-[1(S)-ethoxycarbonyl-3-(1-benzyloxycarbonyl-4-piperidyl)propyl]-L-alanyl-L-proline benzylester

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Technology Process of N-[1(S)-ethoxycarbonyl-3-(1-benzyloxycarbonyl-4-piperidyl)propyl]-L-alanyl-L-proline benzylester

There total 7 articles about N-[1(S)-ethoxycarbonyl-3-(1-benzyloxycarbonyl-4-piperidyl)propyl]-L-alanyl-L-proline benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2942-58-7
diethyl cyanophosphonate

: 16652-71-4
benzyl (2S)-2-pyrrolidinecarboxylate hydrochloride

: 120008-74-4
N-[1(S)-ethoxycarbonyl-3-(1-benzyloxycarbonyl-4-piperidyl)propyl]-L-alanyl-L-proline benzylester

Guidance literature:: With pyridine; formic acid; triethylamine; In N-methyl-acetamide; water;

Reference yield:

: 99197-90-7
ethyl 4-(1-benzyloxycarbonyl-4-piperidyl)-2-oxobutyrate

: 120008-74-4
4-{(R)-3-[(S)-2-((S)-2-Benzyloxycarbonyl-pyrrolidin-1-yl)-1-methyl-2-oxo-ethylamino]-3-ethoxycarbonyl-propyl}-piperidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) molecular sieves, 2) sodium cyanoborohydride / 1) EtOH, 1 h

2: 99percent formic acid / 30 h / 40 °C

3: diethyl phosphorocyanidate, Et₃N / dimethylformamide / 3 h

With formic acid; molecular sieve; diethyl cyanophosphonate; sodium cyanoborohydride; triethylamine; In N,N-dimethyl-formamide;

Reference yield:

: 99197-90-7
ethyl 4-(1-benzyloxycarbonyl-4-piperidyl)-2-oxobutyrate

: 120008-74-4
N-[1(S)-ethoxycarbonyl-3-(1-benzyloxycarbonyl-4-piperidyl)propyl]-L-alanyl-L-proline benzylester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) molecular sieves, 2) sodium cyanoborohydride / 1) EtOH, 1 h

2: 99percent formic acid / 30 h / 40 °C

3: diethyl phosphorocyanidate, Et₃N / dimethylformamide

With formic acid; molecular sieve; diethyl cyanophosphonate; sodium cyanoborohydride; triethylamine; In N,N-dimethyl-formamide;