bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite

Base Information

Chemical Name:bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite
CAS No.:1337529-90-4
Molecular Formula:C₂₅H₄₅O₁₁P
Molecular Weight:552.599
Hs Code.:

Synonyms:bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite

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Technology Process of bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite

There total 5 articles about bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1337878-61-1
bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite borane

: 1337529-90-4
bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In benzene; at 50 ℃; for 22h;
DOI:10.1021/ol2020175

Reference yield:

: 1337529-79-9
13-(3-bromophenoxy)-2,5,8,11-tetraoxatridecane

: 1337529-90-4
bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / diethyl ether; hexane / 5 h / -95 - 0 °C

2: 1H-tetrazole / acetonitrile / 16 h / Reflux

With 1H-tetrazole; n-butyllithium; In diethyl ether; hexane; acetonitrile;
DOI:10.1021/ol2020175

Reference yield:

: 23783-42-8,95507-80-5
tetraethylene glycol monomethyl ether

: 1337529-90-4
bis(2-(2-methoxyethoxy)ethyl) (3-(2,5,8,11-tetraoxatridecan-13-yloxy)phenyl)phosphonite

Guidance literature:: Multi-step reaction with 4 steps

1: trimethylamine hydrochloride; triethylamine / acetonitrile / 3.5 h / 0 - 20 °C

2: potassium carbonate / acetonitrile / 16 h / Reflux

3: n-butyllithium / diethyl ether; hexane / 5 h / -95 - 0 °C

4: 1H-tetrazole / acetonitrile / 16 h / Reflux

With 1H-tetrazole; n-butyllithium; trimethylamine hydrochloride; potassium carbonate; triethylamine; In diethyl ether; hexane; acetonitrile;
DOI:10.1021/ol2020175