(3aR,5R,6R,6aR)-5-[(1S)-1-acetoxybut-3-enyl]-6-benzyloxy-2,2-dimethyl-5-vinyltetrahydrofuro[2,3-d][1,3]dioxole

Base Information

Chemical Name:(3aR,5R,6R,6aR)-5-[(1S)-1-acetoxybut-3-enyl]-6-benzyloxy-2,2-dimethyl-5-vinyltetrahydrofuro[2,3-d][1,3]dioxole
CAS No.:1253800-22-4
Molecular Formula:C₂₂H₂₈O₆
Molecular Weight:388.461
Hs Code.:

Synonyms:(3aR,5R,6R,6aR)-5-[(1S)-1-acetoxybut-3-enyl]-6-benzyloxy-2,2-dimethyl-5-vinyltetrahydrofuro[2,3-d][1,3]dioxole

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Chemical Property of (3aR,5R,6R,6aR)-5-[(1S)-1-acetoxybut-3-enyl]-6-benzyloxy-2,2-dimethyl-5-vinyltetrahydrofuro[2,3-d][1,3]dioxole

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Technology Process of (3aR,5R,6R,6aR)-5-[(1S)-1-acetoxybut-3-enyl]-6-benzyloxy-2,2-dimethyl-5-vinyltetrahydrofuro[2,3-d][1,3]dioxole

There total 1 articles about (3aR,5R,6R,6aR)-5-[(1S)-1-acetoxybut-3-enyl]-6-benzyloxy-2,2-dimethyl-5-vinyltetrahydrofuro[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1253800-18-8
(3aR,5S,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-hydroxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole

: 108-24-7
acetic anhydride

: 1253800-22-4
(3aR,5R,6R,6aR)-5-[(1S)-1-acetoxybut-3-enyl]-6-benzyloxy-2,2-dimethyl-5-vinyltetrahydrofuro[2,3-d][1,3]dioxole

Guidance literature:: In pyridine; at 20 ℃; for 12h;
DOI:10.1055/s-0029-1218828

Reference yield: 79.0%

: 1253800-22-4
(3aR,5R,6R,6aR)-5-[(1S)-1-acetoxybut-3-enyl]-6-benzyloxy-2,2-dimethyl-5-vinyltetrahydrofuro[2,3-d][1,3]dioxole

: 1253800-23-5
C₂₀H₂₄O₆

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1055/s-0029-1218828