C₂₃H₃₀N₂O₈

Base Information

• Chemical Name: C₂₃H₃₀N₂O₈
• CAS No.: 1310929-22-6
• Molecular Formula: C₂₃H₃₀N₂O₈
• Molecular Weight: 462.5
• Mol file: 1310929-22-6.mol

Synonyms:C₂₃H₃₀N₂O₈

Chemical Property of C₂₃H₃₀N₂O₈

Chemical Property:

Purity/Quality:

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Technology Process of C₂₃H₃₀N₂O₈

There total 2 articles about C₂₃H₃₀N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C18H25NO5 (1310929-14-6) + N-α-diazoacetyloxazolidinone → C23H30N2O8 (1310929-22-6)

Guidance literature:

With (S)-[3,3’-diphenyl-1,1’-binaphthalen-2,2’-yl]-N-triflyl phosphoramide; In toluene; at -20 ℃; for 4h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1021/ja203901h

Reference yield:

3-bromoacetyl-1,3-oxazolidin-2-one (141353-28-8) → C23H30N2O8 (1310929-22-6)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N'-ditosylhydrazine; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 16 h / 0 - 20 °C

2: (S)-[3,3’-diphenyl-1,1’-binaphthalen-2,2’-yl]-N-triflyl phosphoramide / toluene / 4 h / -20 °C / Inert atmosphere

With (S)-[3,3’-diphenyl-1,1’-binaphthalen-2,2’-yl]-N-triflyl phosphoramide; N,N'-ditosylhydrazine; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; toluene;

DOI:10.1021/ja203901h

upstream raw materials:

C₁₈H₂₅NO₅

3-bromoacetyl-1,3-oxazolidin-2-one

Refernces