N₄-(4-aminomethyl-cyclohexylmethyl)-N₂-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine

Base Information

• Chemical Name: N₄-(4-aminomethyl-cyclohexylmethyl)-N₂-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine
• CAS No.: 736050-81-0
• Molecular Formula: C₂₀H₂₈N₆O₂S
• Molecular Weight: 416.547

Synonyms:N₄-(4-aminomethyl-cyclohexylmethyl)-N₂-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine

Chemical Property of N₄-(4-aminomethyl-cyclohexylmethyl)-N₂-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine

Chemical Property:

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Technology Process of N₄-(4-aminomethyl-cyclohexylmethyl)-N₂-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine

There total 1 articles about N₄-(4-aminomethyl-cyclohexylmethyl)-N₂-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-methylsulfanyl-benzyl)-(5-nitro-4-thiocyanato-pyrimidin-2-yl)-amine + 1,4-bis-(aminomethyl)cyclohexane (2549-93-1) → N4-(4-aminomethyl-cyclohexylmethyl)-N2-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine (736050-81-0)

Guidance literature:

In dichloromethane; at 20 ℃; for 16h;

DOI:10.1016/j.bmcl.2006.09.056

Reference yield: 22.0%

N4-(4-aminomethyl-cyclohexylmethyl)-N2-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine (736050-81-0) + formaldehyd (50-00-0,30525-89-4,61233-19-0) → N4-(4-dimethylaminomethyl-cyclohexylmethyl)-N2-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine (736047-48-6)

Guidance literature:

With sodium cyanoborohydride; acetic acid; In methanol; water; at 0 - 20 ℃; for 2h;

Reference yield:

N4-(4-aminomethyl-cyclohexylmethyl)-N2-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine (736050-81-0) + 1-(2-(methylthio)phenyl)methanamine (56004-83-2) → N4-(4-dimethylaminomethyl-cyclohexylmethyl)-N2-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine (736047-48-6)

Guidance literature:

With formaldehyd; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; In methanol;

upstream raw materials:

1,4-bis-(aminomethyl)cyclohexane

Downstream raw materials:

N₄-(4-dimethylaminomethyl-cyclohexylmethyl)-N₂-(2-methylsulfanyl-benzyl)-5-nitro-pyrimidine-2,4-diamine

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