Technology Process of C17H22O4
There total 8 articles about C17H22O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C18H26O7S;
With
sodium tetrahydroborate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 8h;
With
dihydrogen peroxide;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
Further stages.;
DOI:10.1016/j.tetlet.2007.07.177
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 81 percent / PhNEt2 / 12 h / 180 °C
2.1: 82 percent / K2CO3 / dimethylformamide / 8 h / 90 °C
3.1: NaOH / methanol / 4 h / 20 °C
3.2: 95 percent / diethyl ether / 2 h / 0 °C
4.1: 91 percent / pyridine / CH2Cl2 / 14 h / 20 °C
5.1: o-NO2-PhSeCN; NaBH4 / dimethylformamide / 8 h / 20 °C
5.2: 80 percent / H2O2 / tetrahydrofuran / 3 h / 20 °C
With
pyridine; sodium hydroxide; sodium tetrahydroborate; potassium carbonate; N,N-diethylaniline;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
1.1: Claisen rearrangement;
DOI:10.1016/j.tetlet.2007.07.177
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: NaOH / methanol / 4 h / 20 °C
1.2: 95 percent / diethyl ether / 2 h / 0 °C
2.1: 91 percent / pyridine / CH2Cl2 / 14 h / 20 °C
3.1: o-NO2-PhSeCN; NaBH4 / dimethylformamide / 8 h / 20 °C
3.2: 80 percent / H2O2 / tetrahydrofuran / 3 h / 20 °C
With
pyridine; sodium hydroxide; sodium tetrahydroborate;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.07.177
