N(sup 1)-acetylspermidine dihydrochloride

Base Information

• Chemical Name: N(sup 1)-acetylspermidine dihydrochloride
• CAS No.: 34450-16-3
• Molecular Formula: C9H21N3O
• Molecular Weight: 260.207
• Mol file: 34450-16-3.mol

Synonyms:Acetamide, N-[3-[(4-aminobutyl)amino]propyl]-, dihydrochloride;N1-Acetylspermidine (hydrochloride);

Chemical Property of N(sup 1)-acetylspermidine dihydrochloride

Chemical Property:

• Vapor Pressure: 5.42E-06mmHg at 25°C
• Melting Point: 184-188°C
• Boiling Point: 380.5°C at 760 mmHg
• Flash Point: 183.9°C
• PSA: 67.15000
• LogP: 2.12520
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature
• Solubility.: Methanol (Slightly, Heated), Water (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

N1-AcetylspermidineDihydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Dihydrochloride salt of N1-Acetylspermidine which is an analog of Spermidine (S680400), an antineoplastic.

Technology Process of N(sup 1)-acetylspermidine dihydrochloride

There total 3 articles about N(sup 1)-acetylspermidine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-acetyl-3-aminopropanaldehyde (73323-68-9) → N1-acetylspermidine dihydrochloride (34450-16-3)

Guidance literature:

Multi-step reaction with 3 steps

1: CH₂Cl₂

2: NaBH₄

3: H₂

With sodium tetrahydroborate; hydrogen; In dichloromethane;

Reference yield:

[4-(3-Acetylamino-propylamino)-butyl]-carbamic acid benzyl ester (86550-26-7) → N1-acetylspermidine dihydrochloride (34450-16-3)

Guidance literature:

With hydrogen; Yield given;

Reference yield:

{4-[3-Acetylamino-prop-(E)-ylideneamino]-butyl}-carbamic acid benzyl ester (86550-24-5) → N1-acetylspermidine dihydrochloride (34450-16-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NaBH₄

2: H₂

With sodium tetrahydroborate; hydrogen;

upstream raw materials:

[4-(3-Acetylamino-propylamino)-butyl]-carbamic acid benzyl ester

N-acetyl-3-aminopropanaldehyde

{4-[3-Acetylamino-prop-(E)-ylideneamino]-butyl}-carbamic acid benzyl ester

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