β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide

Base Information

Chemical Name:β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide
CAS No.:96885-51-7
Molecular Formula:C₂₀H₂₂N₈O₆
Molecular Weight:470.445
Hs Code.:

Synonyms:β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide

Suppliers and Price of β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide

There total 6 articles about β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.7%

: 555-16-8
4-nitrobenzaldehdye

: 96885-50-6
β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionyl hydrazide

: 96885-51-7
β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; water; for 1h; Heating;
DOI:10.1007/BF00768336

Reference yield:

: 77350-93-7
3-methyl-8-chloroxanthine

: 96885-51-7
β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / Et₃N / butan-1-ol / 4 h / Heating

2: 28.3 percent / dimethylformamide / 3 h / Heating

3: 64.2 percent / conc. HCl / 1 h / Heating

4: 73.7 percent / conc. H₂SO₄ / 1.5 h / Heating

5: 95.5 percent / hydrazine hydrate / ethanol / 0.5 h / Heating

6: 95.7 percent / conc. HCl / H₂O; dioxane / 1 h / Heating

With hydrogenchloride; sulfuric acid; hydrazine hydrate; triethylamine; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1007/BF00768336

Reference yield:

: 96885-45-9
3-Methyl-7-(β-cyanoethyl)-8-chloroxanthine

: 96885-51-7
β-(3-Methyl-8-N-morpholino-7-xanthinyl)propionic acid N-(p-nitrobenzylidene)hydrazide

Guidance literature:: Multi-step reaction with 5 steps

1: 28.3 percent / dimethylformamide / 3 h / Heating

2: 64.2 percent / conc. HCl / 1 h / Heating

3: 73.7 percent / conc. H₂SO₄ / 1.5 h / Heating

4: 95.5 percent / hydrazine hydrate / ethanol / 0.5 h / Heating

5: 95.7 percent / conc. HCl / H₂O; dioxane / 1 h / Heating

With hydrogenchloride; sulfuric acid; hydrazine hydrate; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1007/BF00768336