silver salt of 2-[(3S,4R)-3-[(1'R)-1-allyloxycarbonyloxyethyl]-4-mercapto-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester

Base Information

• Chemical Name: silver salt of 2-[(3S,4R)-3-[(1'R)-1-allyloxycarbonyloxyethyl]-4-mercapto-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester
• CAS No.: 104698-13-7
• Molecular Formula: Ag*C₃₂H₃₁NO₆PS
• Molecular Weight: 696.509

Synonyms:silver salt of 2-[(3S,4R)-3-[(1'R)-1-allyloxycarbonyloxyethyl]-4-mercapto-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester

Chemical Property of silver salt of 2-[(3S,4R)-3-[(1'R)-1-allyloxycarbonyloxyethyl]-4-mercapto-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester

Chemical Property:

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Technology Process of silver salt of 2-[(3S,4R)-3-[(1'R)-1-allyloxycarbonyloxyethyl]-4-mercapto-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester

There total 1 articles about silver salt of 2-[(3S,4R)-3-[(1'R)-1-allyloxycarbonyloxyethyl]-4-mercapto-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ silver salt of 2-[(3S,4R)-3-[(1'R)-1-allyloxycarbonyloxyethyl]-4-mercapto-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester (104698-13-7)

Guidance literature:

Reference yield:

silver salt of 2-[(3S,4R)-3-[(1'R)-1-allyloxycarbonyloxyethyl]-4-mercapto-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester (104698-13-7) + p-methoxyphenoxyacetyl chloride (42082-29-1) → 2-[(3S,4R)-3-[(1R)-1-allyloxycarbonyloxyethyl]-4-[4-methoxyphenoxymethylthio)-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester

Guidance literature:

With pyridine; dmap; In dichloromethane;

Reference yield:

5-(tetrazol-1-yl)-valeric acid chloride + silver salt of 2-[(3S,4R)-3-[(1'R)-1-allyloxycarbonyloxyethyl]-4-mercapto-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester (104698-13-7) → 2-[(3S,4R)-3-[(1R)-1-allyloxycarbonyloxyethyl]-4-[5-(tetrazol-1-yl)-pentanoylthio]-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester (117027-59-5)

Guidance literature:

With pyridine; dmap; In dichloromethane; ethyl acetate;

Downstream raw materials:

{(S)-3-((R)-1-Allyloxycarbonyloxy-ethyl)-2-[2-(4,5-dimethyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl)-acetylsulfanyl]-4-oxo-azetidin-1-yl}-(triphenyl-λ⁵-phosphanylidene)-acetic acid allyl ester

2-[(3S,4R)-3-[(1R)-1-allyloxycarbonyloxyethyl]-4-(4-allyloxycarbonylaminophenoxyacetylthio)-2-oxoazetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester

2-[(3S,4R)-3-[(1R)-1-allyloxycarbonyloxyethyl]-4-[N-(4-allyloxycarbonylaminophenyl)-N-(allyloxycarbonyl)-glycylthio]2-oxo-azetidin-1-yl]-2-triphenylphosphoran-ylideneacetic acid allyl ester

2-[(3S,4R)-3-[(1R)-1-allyloxycarbonyloxyethyl]-4-[5-(tetrazol-1-yl)-pentanoylthio]-2-oxo-azetidin-1-yl]-2-triphenylphosphoranylideneacetic acid allyl ester

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