2,6-diphenyltricyclo<3.3.1.0^2,8>nona-3,6-diene, 2,6-diphenylbarbaralane

Base Information

Chemical Name:2,6-diphenyltricyclo<3.3.1.0^2,8>nona-3,6-diene, 2,6-diphenylbarbaralane
CAS No.:106913-96-6
Molecular Formula:C₂₁H₁₈
Molecular Weight:270.374
Hs Code.:

2,6-diphenyltricyclo<3.3.1.0<sup>2,8</sup>>nona-3,6-diene, 2,6-diphenylbarbaralane

Synonyms:2,6-diphenyltricyclo<3.3.1.0^2,8>nona-3,6-diene, 2,6-diphenylbarbaralane

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Chemical Property of 2,6-diphenyltricyclo<3.3.1.0^2,8>nona-3,6-diene, 2,6-diphenylbarbaralane

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Technology Process of 2,6-diphenyltricyclo<3.3.1.0^2,8>nona-3,6-diene, 2,6-diphenylbarbaralane

There total 5 articles about 2,6-diphenyltricyclo<3.3.1.0^2,8>nona-3,6-diene, 2,6-diphenylbarbaralane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 106914-00-5
4,8-dibromo-2,6-diphenylbicyclo<3.3.1>nona-2,6-diene

: 106913-96-6
2,6-diphenyltricyclo<3.3.1.0^2,8>nona-3,6-diene, 2,6-diphenylbarbaralane

Guidance literature:: With copper; zinc; In diethyl ether; for 3h; Heating;
DOI:10.1016/S0040-4020(01)87599-2

Reference yield:

: 16473-11-3
bicyclo[3.3.1]nonane-2,6-dione

: 106913-96-6
2,6-diphenyltricyclo<3.3.1.0^2,8>nona-3,6-diene, 2,6-diphenylbarbaralane

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / diethyl ether; tetrahydrofuran / 15 h / Heating

2: cc H₂SO₄ / acetic acid / 0.08 h

3: 100 percent / N-bromosuccinimide / CCl₄ / 0.75 h / Heating

4: 68 percent / Zn-Cu couple / diethyl ether / 3 h / Heating

With N-Bromosuccinimide; sulfuric acid; copper; zinc; In tetrahydrofuran; tetrachloromethane; diethyl ether; acetic acid;
DOI:10.1016/S0040-4020(01)87599-2

Reference yield:

: 106913-99-9
2,6-diphenylbicyclo<3.3.1>nona-2,6-diene

: 106913-96-6
2,6-diphenyltricyclo<3.3.1.0^2,8>nona-3,6-diene, 2,6-diphenylbarbaralane

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / N-bromosuccinimide / CCl₄ / 0.75 h / Heating

2: 68 percent / Zn-Cu couple / diethyl ether / 3 h / Heating

With N-Bromosuccinimide; copper; zinc; In tetrachloromethane; diethyl ether;
DOI:10.1016/S0040-4020(01)87599-2