phenylmethyl (Z)-4,5-dihydro-N-methoxy-4,4-dimethyl-2-oxazolecarboximidate

Base Information

Chemical Name:phenylmethyl (Z)-4,5-dihydro-N-methoxy-4,4-dimethyl-2-oxazolecarboximidate
CAS No.:856908-46-8
Molecular Formula:C₁₄H₁₈N₂O₃
Molecular Weight:262.309
Hs Code.:

Synonyms:phenylmethyl (Z)-4,5-dihydro-N-methoxy-4,4-dimethyl-2-oxazolecarboximidate

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Chemical Property of phenylmethyl (Z)-4,5-dihydro-N-methoxy-4,4-dimethyl-2-oxazolecarboximidate

Chemical Property:

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Technology Process of phenylmethyl (Z)-4,5-dihydro-N-methoxy-4,4-dimethyl-2-oxazolecarboximidate

There total 4 articles about phenylmethyl (Z)-4,5-dihydro-N-methoxy-4,4-dimethyl-2-oxazolecarboximidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 856908-44-6
2-chloro-N-methoxy-4,4-dimethyl-2-oxazolidinecarboximidoyl bromide

: 100-51-6,185532-71-2
benzyl alcohol

: 856908-46-8
phenylmethyl (Z)-4,5-dihydro-N-methoxy-4,4-dimethyl-2-oxazolecarboximidate

Guidance literature:: benzyl alcohol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.333333h;

2-chloro-N-methoxy-4,4-dimethyl-2-oxazolidinecarboximidoyl bromide; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1248/cpb.53.355

Reference yield:

: 856908-35-5
ethyl 2-chloro-4,4-dimethyl-2-oxazolidinecarboxylate

: 856908-46-8
phenylmethyl (Z)-4,5-dihydro-N-methoxy-4,4-dimethyl-2-oxazolecarboximidate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 62 percent / pyridine / methanol / 24 h / 20 °C

2.1: Ph₃P; CBr₄ / acetonitrile / 3 h / Heating

3.1: NaH / tetrahydrofuran / 0.33 h / 20 °C

3.2: tetrahydrofuran / 4 h / 20 °C

With pyridine; carbon tetrabromide; sodium hydride; triphenylphosphine; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1248/cpb.53.355

Reference yield:

: 856908-42-4
2-chloro-N-methoxy-4,4-dimethyl-2-oxazolidinecarboxamide

: 856908-46-8
phenylmethyl (Z)-4,5-dihydro-N-methoxy-4,4-dimethyl-2-oxazolecarboximidate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Ph₃P; CBr₄ / acetonitrile / 3 h / Heating

2.1: NaH / tetrahydrofuran / 0.33 h / 20 °C

2.2: tetrahydrofuran / 4 h / 20 °C

With carbon tetrabromide; sodium hydride; triphenylphosphine; In tetrahydrofuran; acetonitrile;
DOI:10.1248/cpb.53.355