ethyl (Z)-(2-cyano-2-(2-(2,5-dichlorophenyl)hydrazono)acetyl)carbamate

Base Information

Chemical Name:ethyl (Z)-(2-cyano-2-(2-(2,5-dichlorophenyl)hydrazono)acetyl)carbamate
CAS No.:53366-34-0
Molecular Formula:C₁₂H₁₀Cl₂N₄O₃
Molecular Weight:329.142
Hs Code.:

Synonyms:ethyl (Z)-(2-cyano-2-(2-(2,5-dichlorophenyl)hydrazono)acetyl)carbamate

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Chemical Property of ethyl (Z)-(2-cyano-2-(2-(2,5-dichlorophenyl)hydrazono)acetyl)carbamate

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Technology Process of ethyl (Z)-(2-cyano-2-(2-(2,5-dichlorophenyl)hydrazono)acetyl)carbamate

There total 1 articles about ethyl (Z)-(2-cyano-2-(2-(2,5-dichlorophenyl)hydrazono)acetyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.07%

: 6629-04-5
ethyl N-cyanoacetylcarbamate

: 95-82-9
2,5 dichloroaniline

: 53366-34-0
ethyl (Z)-(2-cyano-2-(2-(2,5-dichlorophenyl)hydrazono)acetyl)carbamate

Guidance literature:: 2,5 dichloroaniline; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 0.5h;

ethyl N-cyanoacetylcarbamate; With sodium acetate; In ethanol; water; at 0 ℃; for 2h;
DOI:10.1016/j.ejmech.2016.04.062

Reference yield: 66.15%

: 53366-34-0
ethyl (Z)-(2-cyano-2-(2-(2,5-dichlorophenyl)hydrazono)acetyl)carbamate

: 2-(2,5-dichlorophenyl)-3,5-dioxo-2,3,4,5-tetrahydro-1,2,4-triazine-6-carbonitrile

Guidance literature:: With sodium acetate; acetic acid; for 2h; Reflux;
DOI:10.1016/j.ejmech.2016.04.062

Reference yield:

: 53366-34-0
ethyl (Z)-(2-cyano-2-(2-(2,5-dichlorophenyl)hydrazono)acetyl)carbamate

: 66707-25-3
2-(2,5-dichloro-phenyl)-4-methyl-3,5-dioxo-2,3,4,5-tetrahydro-[1,2,4]triazine-6-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; sodium acetate / 2 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

2.2: 2 h / 0 °C

With sodium acetate; sodium hydride; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2016.04.062